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487results about How to "Slow reaction speed" patented technology

Ultra-low resistance acid-type microemulsion plugging removal and stimulation technology for low permeability oil well

The invention relates to a plugging removal and stimulation method for a low permeability oil well. The ultra-low resistance acid-type microemulsion is prepared by the following components: 10%-25% of acid, 5%-20% of oil, 5%-25% of alcohol, 0.5%-5% of surfactant, 0.5%-3% of inorganic salt, 0.3-1.5% of corrosion inhibitor and the balance water. The method comprises the following steps: injecting the prepared microemulsion in the oil bearing reservoir of the oil well, closing the oil well to react for 4-10h, cleaning the oil well, flowing the reaction exhaust liquor back, and completing the oilwell to perform normal production. The ultra-low resistance acid-type microemulsion used by the invention has thermodynamic stability, is a high dispersive acid-type microemulsion with good solubilization capacity, has ultra-low surface and interfacial tensions and good solubilization capacity and can increase the dispersive capacity of crude in water and the emulsification and peeling function to oil film; the microemulsion also has good dissolubility in water or oil and good fluidity due to high carrying capability and low seepage resistances so that the oil yield of the oil well is increased and the water content is reduced; the liquid surface tension in oil reservoir is reduced and the flow resistance of the crude is lowered so that the mining rate of the crude is increased and the plugging removal and stimulation of the oil well can be realized.
Owner:陕西中孚石油信息技术有限公司 +1

High-performance epoxy bitumen mixture easy to construct and maintain and preparation method thereof

The invention discloses a high-performance epoxy bitumen mixture easy to construct and maintain, comprising four components of A, B, C and D. The high-performance epoxy bitumen mixture easy to construct and maintain is characterized in that the component A mainly comprises epoxy resin, a toughening agent, an accelerating agent and a diluent agent; the component B mainly comprises a curing agent, an accelerating agent, a compatilizer and a diluent agent; the component C comprises bitumen; the component D comprises aggregates and mineral powder, wherein the ratio of the component A to the component B is 100:50 to 100:100; the ratio of the sum of the component A and the component B to the component C is 100:100 to 100:160; and the ratio of the sum of the component A, the component B and the component C to the component D is 6:94 to 7:93. The high-performance epoxy bitumen mixture easy to construct and maintain has the characteristics of excellent mechanical property, temperature resistance, water resistance, solvent corrosion resistance, fatigue durability, simple construction process and short maintenance time. The high-performance epoxy bitumen mixture easy to construct and maintain is suitable for paving and maintenance of road surfaces, such as steel bridge floors, cement concrete bridge floors, tunnels, expressways and the like. The invention also discloses a preparation method of the high-performance epoxy bitumen mixture easy to construct and maintain.
Owner:NANJING UNIV

Self-born acid composite acid fracturing process for high-temperature deep well carbonate rock reservoir

The invention relates to a self-born acid composite acid fracturing process for a high-temperature deep well carbonate rock reservoir. The process comprises the following work procedures of: (1) injecting slick water into a stratum through an oil pipe; (2) injecting non-crosslinked fracturing liquid into the stratum through the oil pipe; (3) injecting a self-born acid system into the stratum through the oil pipe; (4) injecting a gelled acid system into the stratum through the oil pipe in a low-displacement mode; and (5) injecting the slick water into the stratum through the oil pipe, wherein the volume proportions of liquid, accounting for the total liquid injected into the stratum, injected in the first to fifth work procedures are shown as follows: the slick water in the first work procedure accounts for 3 to 10 percent; the non-crosslinked fracturing liquid in the second work procedure accounts for 40 to 60 percent; the self-born acid system in the third work procedure accounts for 30 to 50 percent; the gelled acid system in the fourth procedure accounts for 3 to 10 percent; the volume proportion of the slick water in the fifth work procedure is 3 to 15 percent; and the volume unit is m<3>. Through the self-born acid composite acid fracturing process, the flow guide capability is improved by more than 140md.m, and the deep penetration effect of the high-temperature deep well carbonate rock reservoir is obvious.
Owner:CHINA PETROLEUM & CHEM CORP

Direct-drive permanent magnet fan harmonic wave suppression optimizing method in asymmetric fault of power grid voltage

The invention discloses direct-drive permanent magnet fan harmonic wave suppression optimizing method in an asymmetric fault of power grid voltage. The method comprises the steps of acquiring abc three-phase static voltage according to abc three-phase current at the motor side; extracting harmonic current by 5-7 times according to the abc three-phase current at the motor side, performing harmonic current suppression, and acquiring abc three-phase compensation voltage; adding the abc three-phase static voltage and the abc three-phase compensation voltage for obtaining a control signal; performing SVPWM modulation on the control signal for obtaining a PWM wave, and controlling an inverter switch of the direct-driven permanent magnet fan through the PWM wave, thereby driving a permanent magnet synchronous generator (PMSG) of the drive-drive permanent magnet fan. According to the method of the invention, through acquiring the abc three-phase compensation voltage after extracting the harmonic current by 5-7 times and performing harmonic current suppression, the abc three-phase static voltage is compensated for generating a control signal, and a harmonic wave component in the motor current on the condition of asymmetric fault can be compensated, thereby greatly reducing influence of DC bus voltage to a motor-side current transformer, improving waveform of the motor current and performing a relatively high harmonic wave suppression effect.
Owner:HUNAN UNIV

Slow blockage removing agent for oil well and blockage removing method

ActiveCN105255466AUnblock pollutionFree from secondary injuryDrilling compositionClay mineralsFluoboric acid
The invention discloses a slow blockage removing agent for an oil well and a blockage removing method, and belongs to the technical field of oil field exploitation. The slow blockage removing agent is prepared from prepad fluid, main fluid and post-pad fluid, the prepad fluid and the post-pad fluid both take hydrochloric acid as the main component of acid fluid for removing inorganic scale precipitation and dissolving reaction residues, and the main fluid takes glacial acetic acid and fluoboric acid as the main components of acid fluid for stabilizing clay mineral of a reservoir stratum, decreasomg the acid rock reaction speed, enlarging the blockage removing radius and increasing the blockage removing depth. For a fracturing production horizontal well, the treatment fluid is injected into the reservoir stratum in the former stage, the intermediate stage and the later stage, and liquid nitrogen is simultaneously injected, so that residual reaction fluid can be quickly drained after blockage removing construction is performed; pollution blockage near a well bore of the oil well can be effectively removed, the effective permeability near the well bore is increased, the individual-well producing rate is increased, damage caused by excessive acid corrosion to the rock framework of the reservoir stratum can be avoided, and therefore the reservoir stratum can be prevented from being subjected to secondary damage.
Owner:CHINA PETROLEUM & CHEM CORP +1

Super-wide-temperature-range nickel-hydrogen battery and manufacturing method therefor

The invention discloses a super-wide-temperature-range nickel-hydrogen battery. The battery comprises an iron shell as well as a nickel electrode, a hydrogen electrode, a diaphragm and an electrolyte solution mounted in the iron shell, wherein the nickel electrode takes foam nickel as a substrate material; the space in foam nickel is filled with a positive electrode active substance Ni(OH)2, a conductive agent, an additive and a binder; the hydrogen electrode takes a porous nickel-plated steel belt, a copper net or foam nickel as a substrate material; the porous nickel-plated steel belt, the copper net or foam nickel is coated with a negative electrode active substance, namely, hydrogen storage alloy powder, the conductive agent, the additive or the binder; and the electrolyte solution is a mixture of a potassium-rich alkaline aqueous solution and sodium tungstate or tungstic acid crystals. The invention furthermore discloses a manufacturing method for the super-wide-temperature-range nickel-hydrogen battery. According to the super-wide-temperature-range nickel-hydrogen battery disclosed by the invention, the ratio of 0.2C discharge capacity to normal-temperature capacity maximally can reach 70-80% in an environment with the temperature of -45 DEG C; and the ratio of 0.2C discharge capacity to normal-temperature capacity of the nickel hydrogen battery maximally can reach 85-95% in an environment with the temperature of 70 DEG C. Moreover, the manufacturing method is simple and suitable for large-scale production.
Owner:HENGYANG BST POWER

Preparation method of multi-component organic cross-linked acid liquid

The invention relates to a preparation method of multi-component organic cross-linked acid liquid, which comprises base liquid and a cross-linking agent, wherein the weight ratio of the base liquid and the cross-linking agent is 100:0.6-0.8; the base liquid comprises the following components in percentage by weight: 3.6-9 percent of formic acid, 4.8-12 percent of acetic acid, 5.5-13.75 percent ofhydrochloric acid, 0.6-0.8 percent of thickening agent, 4.0-5.0 percent of high-temperature corrosion inhibitors, 0.5-1.0 percent of long-term clay stabilizer, 1.0-1.5 percent of ferric ion stabilizers, 0.5-1.0 percent of broken emulsion discharge aiding agent and the balance is water; and the sum of the mass percentages of all the components is 100%. The method has the beneficial effects that the acid liquid system can be cross-linked under the conditions of high temperature and strong acid and is good in temperature resistance and shear resistance, less in filtration and complete in gelout;after the acid liquid is cross-linked, an acid rock is remarkably lower than ordinary gelled acid in reaction speed and is good in speed retarding performance; and the multi-component organic cross-linked acid liquid can be used for realizing the modification of depth acid pressure in a high-temperature deep well of a carbonate rock.
Owner:BC P INC CHINA NAT PETROLEUM CORP +2

Proppant-carrying acid fracturing method for high-temperature ultra-deep carbonate reservoir

The invention provides a proppant-carrying acid fracturing method for a high-temperature ultra-deep carbonate reservoir. The proppant-carrying acid fracturing method for the high-temperature ultra-deep carbonate reservoir comprises the following steps that (1) fracture forming is conducted through fracturing fluid; (2) ground crosslinked acid is adopted and is made to react with rock, so that an acid-etched fracture is generated in a formed fracture, and a proppant is carried with the ground crosslinked acid for supporting the acid-etched fracture; and (3) linear glue is used for replacement, and thus acid fracturing is completed. According to the proppant-carrying acid fracturing method for the high-temperature ultra-deep carbonate reservoir, the technique is simple, operation is convenient, and the construction effect is remarkable; and the proppant-carrying acid fracturing method is suitable for transforming construction of deep well carbonatite at the high temperature of 150-170 DEG C, a supporting fracture which has deep penetration and longer flow conductivity can be formed in a stratum, the productivity is increased and the production time is prolonged after acid fracturing and well fracturing, and the length of the formed fracture is larger than 120 m.
Owner:CHINA PETROLEUM & CHEM CORP +1

Water-soluble asymmetric indocyanine fluorescent dye and preparation method thereof

The invention discloses a water-soluble asymmetric indocyanine fluorescent dye. A general formula of the dye is as shown in the specification, wherein n is equal to 1, 2 or 3. A preparation method comprises the steps that (1), N-(3,5-2(2-(2-methoxyethoxy) oxethyl) oxethyl) benzyl-2,3,3-trimethyl-5-sulfonic group-3H-indole is synthesized; 2,3,3-trimethyl-5-sulfonic group-3H-indole, organic sylvine, and 3,5-2(2-(2-methoxyethoxy) oxethyl) oxethyl) oxethyl benzylbromide are added to an alcohol solvent in sequence, and conduct backflow reaction for 20-40h under inert gas shielding; the solvent is distilled off after the reaction; column separation is conducted; a red solid product is obtained; and (2), N-carboxyl benzyl-2,3,3-trimethyl-5-sulfonic group-3H-indole, the product and a condensing agent are dissolved in an acetic acid/acetic anhydride mixed solvent; pyridine or pyrimidine is added, and reacts at 60-100 DEG C for 1-6h under the inert gas shielding; ethyl acetate is added after the reaction for dissolving out a precipitate; suction filtration is conducted; the product is separated by taking a methanol/acetonitrile mixed solvent as an eluent, and using a reverse phase silica gel filling separation column; three color strips are obtained; the second color strip is accepted; and the water-soluble asymmetric indocyanine fluorescent dye is obtained.
Owner:HENAN UNIVERSITY

Chemical cleaning method for nanofiltration or reverse osmosis membranes

InactiveCN109224870AExtended service lifeImprove clear liquid handling capacitySemi-permeable membranesReverse osmosisNanofiltration
The invention discloses a chemical cleaning method for nanofiltration or reverse osmosis membranes. The chemical cleaning method includes the following steps: (1) pickling the nanofiltration or reverse osmosis membranes by acidic solutions; (2) cleaning the nanofiltration or reverse osmosis membranes by product water after pickling; (3) performing alkali washing on the nanofiltration or reverse osmosis membranes by alkaline cleaning solutions; (4) cleaning the nanofiltration or reverse osmosis membranes by the product water after alkali washing to complete cleaning of the nanofiltration or reverse osmosis membranes. The chemical cleaning method has the advantages that various pollutants on the nanofiltration or reverse osmosis membranes can be efficiently removed, the operating pressure ofthe nanofiltration or reverse osmosis membranes can be reduced, the yield of clear liquid of the nanofiltration or reverse osmosis membranes can be increased, the service life of the nanofiltration or reverse osmosis membranes can be prolonged, the power consumption of the clear liquid can be lowered, and stable operation of landfill leachate treatment plants can be guaranteed; the chemical cleaning method has the advantages of simple process, convenience in operation, low cleaning cost, high cleaning efficiency, good cleaning effect, high application value, good application prospect and thelike.
Owner:HUNAN JUNXIN ENVIRONMENTAL PROTECTION CO LTD
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