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219results about How to "High content of active substances" patented technology

Preparation method of silicon and carbon-coated graphene composite cathode material

ActiveCN103050666ARealize in situ restorationThe preparation process is simple, convenient and practicalMaterial nanotechnologyCell electrodesCarbon coatedStructural stability
The invention discloses a preparation method of a silicon and carbon-coated graphene composite cathode material. The technical problem to be solved is to enhance the electronic conductivity of the silicon-based cathode material, buffer the volume effect produced in the process of deintercalation of the lithium in the silicon-based cathode material and enhance the structure stability in the circulation process of the material at the same time. The material is prepared by using a spray drying-thermally decomposing treatment process in the invention. The preparation method comprises the following steps of: evenly dispersing nano silicon and graphite micro powder in a dispersion solution of oxidized graphene, carrying out thermal treatment under an inert protection atmosphere after spray drying, subsequently cooling along a furnace to obtain the silicon and carbon-coated graphene composite cathode material. The extra binder does not need to add in the process of manufacturing balls in the invention and the outer oxidized graphene is thermally reduced in situ to graphene in the thermal treatment process of the composite precursor, so that the process is simple and easy to operate; and the practical degree is high. The prepared composite material has the advantages of great reversible capacity, designable capacity, good cycling performance and high-current discharging performance, high tap density and the like.
Owner:CENT SOUTH UNIV

Phosphate material having mesoporous structure for lithium secondary batteries and preparation method thereof

The invention relates to a phosphate material having a mesoporous structure for lithium secondary batteries and a preparation method thereof. The material having a mesoporous structure is secondary particles which have a mesoporous spherical or spheroid shape and are formed by the agglomeration of primary particles; the chemical composition of the material having the mesoporous structure is represented by the formula of LixAaMmBbPOzNn; the average particle diameter of the primary particles is 10nm to 1mum, the average particle diameter of the secondary particles is 100nm to 50mum, the average pore diameter of mesopores is 2 to 500nm; and the material having the mesoporous structure also comprises a layer of 2 to 100nm thick carbon coated outside the secondary particles and on the inner walls of the mesopores, wherein the content of the carbon accounts for 1 to 20 weight percent of the total weight of a substrate. The material is prepared by the steps of: firstly preparing pure-phase phosphate LiMPO4 or doped LiMPO4 sol; secondly, forming dry gel through heat treatment; and finally, forming the agglomerate secondary particles through sintering at high temperature. The phosphate material having the mesoporous structure can be directly used in secondary lithium batteries as an anode active material and can also be used by being mixed with the prior anode material as an additive. The material having the mesoporous structure can improve the rate performance and energy density of the prior anode material and batteries. The secondary lithium batteries containing the phosphate material having the mesoporous structure has high power density and high safety.
Owner:INST OF PHYSICS - CHINESE ACAD OF SCI

Method for preparing seaweed extracting solution and rotation basket extracting device

The invention provides a method for preparing a seaweed extracting solution and a rotation basket extracting device. The preparing method includes the steps that seaweed and activated carbon are thrown into a plurality of medicine baskets, and meanwhile solvent is added into a tank body; a motor is started, a center shaft is made to rotate, hence, the medicine baskets are driven to make centrifugal movement, and chemical substances included in the seaweed are extracted through the solvent; after extracting is completed, the extracting solution is discharged from a liquid medicine outlet; the extracting solution is settled through kieselguhr; supernate is collected, microfiltration is conducted through a ceramic membrane, permeate liquid is collected, and accordingly the seaweed extracting solution is obtained. The rotation basket extracting device comprises the tank body, the center shaft and the medicine baskets. The center shaft penetrates in the center of the tank body in a rotating mode, the medicine baskets are arranged on the center shaft, solvent inlets and a medicine change opening are formed in the top of the tank body, and the liquid medicine outlet is formed in the center of the bottom of the tank body. The method has the advantages of being simple in process, short in period, environmentally friendly and safe. The content of active substances of the prepared extracting solution is high, the number of varieties of active ingredients is large, and stability is achieved.
Owner:SHANGHAI FOREST CABIN BIOLOGICAL TECH

Porous manganese phosphate lithium-carbon composite material and preparation method

The invention discloses a porous manganese phosphate lithium-carbon composite material and a preparation method. The composite material comprises a manganese phosphate lithium material and 1%-15wt% of carbon element, a composition general formula of the manganese phosphate lithium material is LiMnxFe1-xPO4, wherein 0.6<=x<=1, and the particle size of the composite material is 1-50 mum, a plurality of holes with 3-50nm of aperture is provided in the composite material, the material thickness between the adjacent holes is 20-70nm, and the preparation method comprises the following steps: mixing porous Mn2P2O7 with ferric salt, a lithium source, phosphate and a carbon source, performing ball milling by a wet method, drying to prepare a reaction precursor, under protective atmosphere, and performing constant temperature calcination on the reaction precursor for 1-30h at the temperature of 500-900 DEG C to obtain the target product. The porous manganese phosphate lithium-carbon composite material has the advantages that 1) the composite material is the micron order manganese phosphate lithium material having nano holes, when the composite material is taken as lithium ion batteries cathode materials for using, the composite material has high specific capacity, rate capability and tap density; and 2) the composite material has the advantages of simple preparation method, low carbon content and high active substance content.
Owner:中科致良新能源材料(浙江)有限公司

Preparation method of compound fertilizer dedicated to ginkgo trees by using blue-green algae as base material

The invention relates to a preparation method of a compound fertilizer dedicated to ginkgo trees, in particular to a preparation method of the compound fertilizer dedicated to ginkgo trees by using blue-green algae as a base material, belonging to the technical field of fertilizers. The preparation method comprises the steps of squeezing blue-green algae to remove excessive moisture to obtain wet blue-green algae, sequentially adding water, cellulase and protease in parts by weight, mixing uniformly, heating, carrying out enzymolysis, and performing enzyme deactivation to obtain enzymatic hydrolysate; adding potassium sulphate in the enzymatic hydrolysate, heating, keeping the temperature for 3-5h, cooling, and carrying out vacuum concentration to obtain concentrated solution; adding sodium humate, potassium humate, ammonium bicarbonate, phosphogypsum, potassium citrate, zinc sulfate, amino acid, polyvinyl alcohol, cellulose and calcium carbide in the concentrated solution, stirring uniformly, spray-drying, and then granulating to obtain a product. The compound fertilizer dedicated to the ginkgo trees can enable the ginkgo trees to have higher stems and more leaves and have high content of active substances.
Owner:南通市通州区五接农业机电管理站有限公司

Method for preparing Chinese caterpillar fungus extracting concentrated liquid and application thereof

The invention belongs to the medicine, processing and healthcare food technical field of cordyceps sinensis, particularly relating to a preparation method of the cordyceps sinensis extractive concentrated solution got by hirsrtella sinensis or hirsutella hepialid and applications of the cordyceps sinensis extractive concentrated solution in preparation of various preparation forms of medicine or healthcare products for strengthening and regulating immunity; thereby the solution can be applied for treating deficiency in lung and kidney, cancers and for helping strengthening immunity after themotherapy. The preparation of the invention is that the hirsrtella sinensis is fermented to produce cordyceps sinensis which is extracted respectively by ethanol, water and zymohydrolysis and then the extractive is condensed into concentrated solution which is produced into various preparation forms by spray-drying or directly produced into soft capsules after sterilization, and then the finished product is prepared well after packing and inspecting. No additive is added into the finished product which is composed of the extractive concentrated solution by 100 per cent. The various preparations prepared by the extractive concentrated solution of cordyceps sinensis all have multiple functions of restoring the deficiency in lung and kidney, strengthening immunity and enhancing resistance and have the function of regulating and steadying the immunological system of a human body, not only applicable to sub-healthy people for regular health care but also evident in efficacy for people who takes organ transplantation, cancer radiotherapy and chemotherapy, pneumonia, hepatitis, chronic nephritis and valetudinarianism.
Owner:叶天任

Method for preparing oil-acyl lysine sodium and composition comprising surfactant through phase-transfer catalysis

The invention discloses a method for preparing oil-acyl lysine sodium and a composition comprising the surfactant through phase-transfer catalysis, belonging to the technical field of fine chemical engineering. According to the technology for synthesizing an oil-acyl lysine sodium type surfactant provided by the invention, oil and lysine sodium are reacted to generate the oil-acyl lysine sodium in the presence of phase-transfer catalysts PEG8000. The method is high in yield and high in raw material utilization rate, the phase-transfer catalysts PEG8000 refer to matrix raw materials and active ingredients of detergents, cosmetics and medicines and has the effects of regulating the viscosity, stabilizing and moisturizing, the product does not need to be separated and purified and can be directly used, the product is a composition of acyl lysine sodium homolog of different carbon chains, the surfactant combination principle is met, the synergistic effect can be achieved, the content of active matters is high, the surface activity is high, the synthetic route is simple, the pollutants are avoided, and the method is an environment-friendly synthetic method. The invention also discloses a surfactant composition comprising the oil-acyl lysine sodium.
Owner:BEIJING TECHNOLOGY AND BUSINESS UNIVERSITY

Lithium-sulfur battery composite positive electrode active material and preparation and application thereof

The invention relates to a novel lithium-sulfur battery positive electrode material. More specifically, the invention relates to a lithium-sulfur battery composite positive electrode active material.The material comprises a plurality of template etching holes, porous carbon with a through hole structure, a vanadium selenide nanosheet filled in a pore cavity of the porous carbon in situ, and an elemental sulfur source. The invention also provides preparation and application of the material. According to the material of the invention, the vanadium selenide material serving as a conductive substrate in the charge-discharge interval of the lithium-sulfur battery can contribute a part of capacity through intercalation reaction; meanwhile, the vanadium selenide material can greatly improve theproblem of large liquid absorption capacity of a traditional porous carbon substrate material, and the liquid sulfur ratio of the lithium-sulfur battery is remarkably reduced; and, in addition, vanadium selenide can improve the adsorption capacity of the carbon substrate to polysulfide and efficiently catalyze conversion of polysulfide, and the shuttle effect is inhibited in cooperation with porous carbon. Therefore, the lithium-sulfur battery according to the present invention has high energy density and good high-rate discharge, and reprents excellent discharge capacity and lifespan characteristics.
Owner:CENT SOUTH UNIV
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