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47results about How to "Suitable for commercial mass production" patented technology

Refining method of crystal type A azilsartan

The invention relates to the field of medicine, and discloses a refining method of crystal type A azilsartan. The method comprises the following steps: S1, mixing ethyl acetate and absolute ethyl alcohol, heating, and then adding an azilsartan crude product, stirring to be completely dissolved, carrying out filter-pressing; S2, stirring the filtrate in the S1 at 20-25 DEG C to crystallize, filtering, granulating the filter residue through a 24-mesh sieve; drying the raw materials by use of a boiling drying and gradient warming way; drying for 50-70min at an ambient temperature condition, and then drying for 50-70min after warming 40+ / -2 DEG C, wherein the granularity control D (90) is 300-400 microns; drying for 2-3h after warming to 50+ / -2 DEG C, and the granularity control D (90) is 100-200 microns, cooling to obtain an azilsartan finished product. By use of the refining method disclosed by the invention, the dosage of a required organic solvent in refining is greatly reduced; and meanwhile, the stable crystal type A azilsartan is obtained since the raw materials are dried by use of the boiling drying and gradient warming way, the refining yield of 90% or above is acquired, the purity is 99.7% or above, the solvent residue (ethyl alcohol) is less than 0.3%, and the drying time is shortened to 3-6h.
Owner:湖南千金湘江药业股份有限公司

Preparation method of high-conductivity solid-state battery electrolyte for energy storage charging system battery

The invention provides a preparation method of a high-conductivity solid-state battery electrolyte for an energy storage charging system battery, which comprises the following steps of (1) weighing lithium oxide, lanthanum oxide (La2O3) and zirconium oxide (ZrO2) as raw materials according to the mass ratio of (7-7.8): 3: 2, mixing to obtain a mixture, and performing ball milling on the mixture by using a high-speed ball mill to obtain mixed powder A, (2) putting the mixed powder A obtained in the step (1) into a crucible, putting the crucible into an atmosphere furnace, sintering, naturally cooling to obtain garnet type electrolyte Li7La3Zr2O12 (LLZO) precursor powder, taking out the precursor powder, and carrying out high-speed ball milling at the same rotating speed and time as that in the step (1) to obtain powder B, and (3) pressing the powder B obtained in the step (2) into an electrolyte sheet by using a tablet press, then putting the electrolyte sheet into a crucible, carrying out landfill sintering by using mother powder, and cooling to room temperature through two-stage sintering to obtain the LLZO solid electrolyte, so that the technical problem of low conductivity of the battery electrolyte of the energy storage charging system can be solved.
Owner:GUANGXI UNIVERSITY OF TECHNOLOGY

Fuel cell anode catalyst and preparation method and application thereof

ActiveCN111668501AHighly alkaline HOR activityImprove stabilityCell electrodesPtru catalystColloidal synthesis
The invention provides a fuel cell anode catalyst and a preparation method and application thereof. According to the preparation method, transition metal is used as a metal source, trioctylphosphine oxide is used as a reaction solvent, a reaction product is prepared through a colloid synthesis method, and then the reaction product and a carbon carrier are subjected to a load reaction to obtain theload type transition metal phosphide anode catalyst. The anode catalyst has high-alkalinity HOR activity and high stability, is relatively low in preparation cost, is suitable for commercial mass production, and has a huge application prospect in the field of fuel cells. Specifically, ruthenium acetylacetonate is used as a ruthenium source, trioctylphosphine oxide is used as a reaction solvent, and tri-n-octylphosphine is used as a phosphorus source. The anode catalyst Ru2P/C is prepared according to the preparation method. When the loading capacity of the anode catalyst Ru2P/C is 0.4mgcm<-2>, the peak power of 1.3Wcm<-2> (the current density is 3.0Acm<-2>) can be achieved under the conditions of 80 DEG C and the back pressure of 0.1Mpa. The mass ratio exchange current density (j<0, m>) of the anode catalyst Ru2P/C is 0.27mAmug<-1>, the area ratio exchange current density (j<0, s>) of the anode catalyst Ru2P/C is 0.37mAcm<-2>, and the mass ratio exchange current density and the area ratio exchange current density of the anode catalyst Ru2P/C respectively reach three times of those of the Ru/C.
Owner:SUZHOU INSTITUE OF WUHAN UNIV

Novel lithium-sulfur battery material applied to energy storage system

The invention provides a novel lithium-sulfur battery material applied to an energy storage system, a preparation method adopting nitrogen-doped porous carbon fiber composite sulfur as a positive electrode material and a positive electrode plate of the positive electrode material. The preparation method of the composite positive electrode material comprises the following steps: mixing a polyethylene oxide-polypropylene oxide-polyethylene oxide triblock copolymer, tetraethyl orthosilicate, ethanol, concentrated hydrochloric acid and cyanoguanidine according to a molar ratio of (0.001-0.01): (0.03-0.4): (0.6-1): (0.01-0.1): (0.01-0.5), and stirring until the raw materials are completely dissolved to obtain a solution N; evaporating the solution N to dryness, and heating to obtain a sample E; cooling the product E, adding the product E into an acid solution for etching, and performing suction filtration and evaporation to dryness to obtain nitrogen-doped porous carbon nanofibers; and mixing the nitrogen-doped porous carbon nanofiber with elemental sulfur to obtain the elemental sulfur loaded nitrogen-doped porous carbon nanofiber composite positive electrode material. The material can solve the technical problems of low conductivity of battery positive elemental sulfur and short charge-discharge cycle life of the battery caused by dissolution of polysulfide in electrolyte.
Owner:GUANGXI UNIVERSITY OF TECHNOLOGY

Preparation method and application of a hydrogel-modified highly stable carbon-based holographic disc

A preparation method and application of a hydrogel-modified highly stable carbon-based holographic disc relates to the field of information storage technology, and solves the problem of a preparation method for a storage medium with high information storage stability and high diffraction efficiency, including in Prepare a porous titanium dioxide film on a disc-shaped glass substrate; immerse in a carbon quantum dot solution to load the porous titanium dioxide film with carbon quantum dots to obtain a carbon quantum dot / titanium dioxide composite film; immerse in a silver nitrate solution and prepare by irradiating with an ultraviolet lamp Silver / carbon quantum dots / titanium dioxide composite film; a layer of hydrogel is attached by pulling dipping method. The preparation method of the present invention is convenient and reliable, low in cost, and suitable for commercial mass production, and the prepared optical disk has the performance advantages of high stability, high efficiency and high uniformity of information storage, which makes holographic optical storage stand out in the field of future data storage. Possibly, it can be well applied to the field of holographic data storage.
Owner:NORTHEAST NORMAL UNIVERSITY
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