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77results about How to "Uniform and stable properties" patented technology

Homogeneous method for preparing wood fiber derivative under room temperature

The invention discloses a homogeneous method for preparing a wood fiber derivative under room temperature. The method comprises the following steps: drying ground wood fiber powder, suspending the dried wood fiber powder in a solvent, and stirring till the wood fiber is dissolved completely to obtain wood fiber solution; dissolving an acylation reagent in the same solvent, and stirring under the room temperature till the acylation reagent is dissolved completely to obtain acylation reagent solution; adding the acylation reagent solution into the wood fiber solution, and carrying out esterification reaction under the room temperature and a moisture isolated condition; and depositing the solution obtained after the esterification reaction, collecting, washing, freezing and drying deposits, and preparing to obtain the required wood fiber derivative. The invention has the advantages that homogeneous derivatization of wood fiber is realized under the room temperature; and not only can the homogeneity and the stability of the product be improved effectively, but also equipment requirements and energy requirements can be reduced. Therefore, the invention has a significant scientific value and practical significance on the development and the utilization of renewable resources such as wood fiber, biological substances and the like.
Owner:广西南宁绿园北林木业有限公司

Method for preparing high performance Ti3AIC2 ceramic powder

The invention relates to a method for preparing high performance Ti3AIC2 ceramic powder, comprising the following steps: Ti powder, Al powder and C powder are provided with the mol ratio of Ti3AIC2 chemical formula featuring Ti:Al:C equaling to 3:1:2; additive NaF is added by superaddition method to control purity of Ti3AIC2; NaF recruitment is 0.5-20wt.% of the total quality of Ti powder, AI powder and C powder; the material and additive powder are placed in a ball-milling jar, absolute ethyl alcohol is added to the ball-milling jar for carrying out wet mixing for 4-12 hours; material powder is obtained either by natural drying or by baking at the temperature of 60-80 DEG C; the material powder is placed in a cylindrical-tile-shaped material boat and in a combustion synthesis system, titanium carbon mixture is placed at an ignition part in front of the material powder as ignition powder; with the protection of argon, electrified tungsten filament ring is used for igniting the reactant, after natural cooling, the obtained product is Ti3AIC2 powder. The invention is characterized by rapid reaction, simple process, low cost, direct use of low-melting-point material as the material of the reactant, no generation of melting and reunion thereof, uniform reaction course, easy control and uniform and stable property of the synthetized Ti3AIC2.
Owner:HONGHE COLLEGE +1

Process for producing monodisperse polymer/calcium carbonate composite fine particle

The invention belongs to the technical field of an organic and inorganic composite material, in particular to a method for preparing monodisperse polymer / calcium carbonate composite particles. The method comprises the following steps: a glass apparatus is pretreated, a polymer solution the concentration of which is between 0.001 and 10 grams per liter is prepared, and 0.001-1 mol / liter calcium salt is added into the polymer solution to prepare a calcium salt / polymer mixture; the mixture stands, the pH value of the mixture is adjusted to between 6 and 13, and 10<1> to 10<3> milliliters of the mixture is taken out and filled into a beaker; a beaker with grinded carbonate is arranged inside a sealing system at a temperature of between 10 and 60 DEG C, and a layer of film is coated on the beaker to control the speed of decomposition and generation of carbon dioxide; a layer of film is coated on a mouth of the beaker which is filled with the mixture, and is provided with a plurality of holes by a pin, and the beaker is placed into the sealing system, reacts for 0.5 hours to 15 days, is taken out for separation of products; and the products are separated and dried to obtain the required products. The raw materials have wide sources and low cost; the solvent adopted has small pollution and no toxic action; and the preparation method is simple and easy to operate, accords with the requirement of green chemistry, and has the potential of large-scale production.
Owner:FUDAN UNIV

Waterborne UV (Ultraviolet) furniture coating and preparation method thereof

The invention discloses a preparation method of waterborne UV (Ultraviolet) furniture coating. The preparation method comprises the following steps: firstly, conveying a waterborne acrylate pre-polymer and an active diluting agent into a high-pressure reaction kettle; introducing carbon dioxide and enabling carbon dioxide to be at a supercritical fluid state through adjusting pressure and temperature in the high-pressure reaction kettle; keeping the pressure and temperature in the high-pressure reaction kettle unchanged; adding other auxiliary agents in sequence according to the ratio; sufficiently stirring and reacting to obtain a finished product. The waterborne UV furniture coating prepared by the method has the advantages of easiness for controlling the viscosity, good storage stability, convenience for construction, green and environment-friendly preparation technology and high production efficiency; the waterborne UV furniture coating can be completely dried after being irradiated through an ultraviolet lamp for several seconds; a dried paint film has high rigidity, good toughness, good water resistance, good wearing resistance, good pollution resistance and good plumpness; all indexes meet national standards, and a decoration effect and a protection effect are strong; the waterborne UV furniture coating has a good adhesive force on various base materials and is applicable to coating of various high-end indoor wood furniture and indoor wood floors.
Owner:安徽科纳家居饰材有限公司

Amphiphilic anti-freeze molecule based on silsesquioxane, preparation method thereof and anti-icing surface material

The invention provides an amphiphilic anti-freeze molecule based on silsesquioxane, a preparation method thereof and an anti-icing surface material and belongs to the technical field of anti-icing surface materials. The invention solves the problem of an instable anti-icing effect of an anti-icing surface material in the prior art. The amphiphilic anti-freeze molecule is prepared by combining the silsesquioxane with an anti-freeze protein or an anti-freeze polypeptide. The invention also provides the preparation method of the amphiphilic anti-freeze molecule based on silsesquioxane. The method includes the steps of preparing the silsesquioxane having reactive groups and hydrophobic groups, and performing a coupling reaction to combine the silsesquioxane with an anti-freeze protein or anti-freeze polypeptide to prepare the amphiphilic anti-freeze molecule based on the silsesquioxane. The invention also provides the anti-icing surface material prepared from the amphiphilic anti-freeze molecule based on the silsesquioxane. The anti-icing surface material has the anti-icing characters of both a hydrophobic material and a hydrophilic material, enlarges a temperature window of the anti-icing surface material and is improved in anti-icing performance.
Owner:CHANGCHUN INST OF APPLIED CHEMISTRY - CHINESE ACAD OF SCI

Method for causticizing corn starch

The invention provides a method for causticizing corn starch, which is characterized in that under the condition that the temperature of corn starch feeding water is 40-50 DEG C, materials are simultaneously fed and stirred, and after material feeding is completed, the obtained mixture is fully and uniformly mixed so as to form a suspension liquid; a sodium hydroxide solution with weight and volume percentages of 20% is added into the suspension liquid, and then a sodium hydroxide solid is added into the obtained substance, wherein the mass ratio of the sodium hydroxide solid to corn starch is 4:100; after the temperature of the obtained mixture rises to 65-75 DEG C, the obtained mixture is causticized for one hour; and after water is added into the causticized mixture for constant volume, a corn starch solution is obtained, and then subjected to heat preservation for later use. The corn starch solution prepared by using the method for causticizing corn starches disclosed by the invention is uniform and stable in properties, easy to store and uneasy to go bad; in case that the corn starch solution is used as an iron mineral inhibitor, no 'clustering' phenomenon occurs in the process of preparation, so that the starch utilization rate is high; and the consumption of a beneficiation reagent is reduced by over 5%, and because the causticizing temperature is lowered, the energy consumption is reduced.
Owner:ANSTEEL GRP MINING CO LTD
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