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A method for preparing carbon quantum dots by using oily sludge
Pending
CN122166764A
Effective peeling
high purity
Nanooptics
Nano-carbon
Sludge
Components of crude oil
This invention relates to the field of harmless treatment technology for oily
sludge
, specifically to a method for preparing
carbon quantum dots
from oily
sludge
. Conventional methods for preparing
carbon quantum dots
from oily
sludge
have limitations in yield and
fluorescence
intensity. To address these issues, this invention provides a method for preparing
carbon quantum dots
from oily sludge. Considering the complex composition of oily sludge, this invention designs a multi-stage purification process chain of "ultrasonic extraction—
water washing
—Soxhlet extraction—
acidification treatment
." Each step works synergistically, purifying the sludge step by step to ultimately obtain a high-purity refined organic
carbon source
. The refined organic
carbon source
removes impurities through gentle
solvent
extraction and
acid washing
, maximizing the preservation of the organic
carbon source
's
chemical activity
and
structural integrity
. In the
hydrothermal reaction
, it can be effectively converted into carbon
quantum
dots, avoiding carbon source loss or activity reduction due to over-
processing
, thus further improving the yield and
fluorescence
intensity of carbon
quantum
dots.
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Owner:
CHANGZHOU UNIV
A method for preparing pyridazine compounds
Pending
CN122256452A
avoid dependence
Become carbon neutral
Microorganism based processes
Fermentation
Furan
Pyridazine
The application belongs to the field of
green manufacturing
, and discloses a preparation method of a
pyridazine
compound, comprising the following steps: (1) adding an
enzyme
catalyst, a bio-based
furan
and a co-substrate into a
buffer solution
to react, and removing cells after the reaction; (2) adding
hydrogen
peroxide
or an oxidase and a
titanium
-
silicon
molecular sieve
to react, and removing the
titanium
-
silicon
molecular sieve
after the reaction; (3) slowly adding hydrazine under stirring at 0-60 DEG C to obtain the
pyridazine
compound after the reaction; the
enzyme
catalyst is at least one of the following: an
alcohol
dehydrogenase
/
glucose dehydrogenase
double
enzyme
system
, an
alcohol
dehydrogenase
/
formate
dehydrogenase
double
enzyme system
and a recombinant bacterium co-expressing one or both of the above two double enzyme systems. The application has the advantages of
high selectivity
, mild
reaction conditions
, environmental friendliness, fast
reaction speed
and no need for intermediate separation and purification.
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Owner:
SOUTH CHINA UNIV OF TECH
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