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110results about How to "Dense growth" patented technology

Preparation method and application of g-C3N4-Cu2O composite catalyst

The invention mainly aims at providing a preparation method and application of a g-C3N4-Cu2O composite catalyst. The preparation method comprises the following steps: providing a first solution, wherein the first solution contains Cu<2+> in a dissolved state; adding protonated g-C3N4 into the first solution, stirring, and carrying out ultrasonic treatment to obtain suspension; adding xylitol into the suspension in a stirring state, adjusting the pH value to 10-12, and stirring to obtain mixed liquid; heating the mixed liquid to 150-200 DEG C in a high-pressure reaction container, and carrying out a reaction for 25-35h at the constant temperature to obtain reactants; cooling the reactants and then carrying out solid-liquid separation on the cooled reactants to obtain a solid product, cleaning, and carrying out vacuum drying; heating the solid product up to 150-250 DEG C under the condition of gas protection, and maintaining the constant temperature for 1-3h to obtain the g-C3N4-Cu2O composite catalyst. The g-C3N4-Cu2O composite catalyst has higher visible absorption capacity and good photocatalytic performance. The g-C3N4-Cu2O composite catalyst can be used for carrying out catalytic treatment on organic pollutants in waste water in presence of visible light, and is remarkable in degradation effect and relatively stable.
Owner:WUHAN TEXTILE UNIV

Bimetallic nitrogen doped carbon/molybdenum disulfide composite electrocatalyst material, preparation method thereof and application thereof

The invention relates to a bimetallic nitrogen doped carbon / molybdenum disulfide composite electrocatalyst material and a preparation method thereof. The preparation method of the bimetallic nitrogendoped carbon / molybdenum disulfide composite electrocatalyst material comprises the following specific steps of 1) preparing bimetallic nitrogen doped carbon: preparing a mixed solution of a zinc salt,a cobalt salt and dimethylimidazole from absolute methanol as a solvent to prepare a bimetallic organic framework; and after calcining the bimetallic organic framework at a high temperature, preparing the bimetallic nitrogen doped carbon; and 2) preparing a bimetallic nitrogen doped carbon / molybdenum disulfide composite material by using a hydrothermal method: preparing a mixed solution of sodiummolybdate etrahydrate and thiocarbamide from deionized water as a solvent; and placing the mixed solution and the bimetallic nitrogen doped carbon into a polytetrafluoroethylene high pressure vesselto perform hydrothermal reaction so as to prepare the bimetallic nitrogen doped carbon / molybdenum disulfide composite material. The bimetallic nitrogen doped carbon / molybdenum disulfide composite electrocatalyst material, provided by the invention, has the advantages that excellent catalytic activity and high stability are shown when the prepared composite material is used for electrocatalytic hydrogen evolution reaction, the preparation cost is low, the repeatability is high, and the application prospect is broad.
Owner:JIANGSU UNIV OF SCI & TECH +1

Preparation method for positive electrode active material, and positive electrode active material

For overcoming the problems of irregular shape, uneven element distribution and partial agglomeration of metal elements of a positive electrode active material prepared by a method in the prior art, the invention provides a preparation method for the positive electrode active material, comprising the steps of S1, mixing a reaction seed crystal with a complexing agent solution, wherein the reaction seed crystal is hydroxide of one or more of nickel, cobalt, manganese or aluminum; and the D50 of the reaction seed crystal is less than or equal to 2-6 [mu]m; S2, under a condition of stirring and ultrasonic processing, adding a metal salt solution and a precipitator solution, regulating PH to 9-13; and then washing and drying to obtain a precursor, wherein the metal salt solution is a solution containing nickel salt, cobalt salt, manganese salt and aluminum salt; and S3, mixing the precursor with a lithium source, performing heat preservation at a temperature of 500-950 DEG C for 2-24h, and cooling. Meanwhile, the invention also discloses the positive electrode active material prepared by the method. The positive electrode active material provided by the invention is regular in shape, high in degree of sphericity, uniform in element distribution and free of partial agglomeration of metal elements; and in addition, the positive electrode active material is high in cycling performance, thermal stability and security.
Owner:BTR NEW MATERIAL GRP CO LTD

Poly(ether-ether-ketone)/nano hydroxyapatite dental implant and manufacturing method thereof

The invention provides a poly(ether-ether-ketone) / nano hydroxyapatite dental implant which consists of a neck part and a root part, wherein the matrix material of the dental implant is a poly(ether-ether-ketone) / nano hydroxyapatite composite material; fibronectin or basic fibroblast growth factors are grafted to the neck part; a sub-surface layer of the root part has a micron porous-nano bulge multistage microstructure; and the surface layers of the neck part and the root part are nano hydroxyapatite layers containing Ag<+> and Zn<2+>. The manufacturing method comprises the following steps: (1) preparing a blank; (2) grafting the fibronectin or basic fibroblast growth factors on the surface of the neck part of the blank; (3) soaking the root part of the blank into a decafluoro-naphthalene solution to etch for 0.5-1 hour, and then putting the blank into nano hydroxyapatite powder to adhere a layer of nano hydroxyapatite particles; and (4) soaking the root of the blank in nano hydroxyapatite slurry doped with Ag<+> or Zn<2+> for 1-3 hours. The poly(ether-ether-ketone) / nano hydroxyapatite dental implant provided by the invention ensures that the elastic modulus of the dental implant is matched with human bone tissues, and the dental implant has high bioactivity and continuous antibacterial ability and can improve the long-term success rate of implantation.
Owner:SICHUAN UNIV

Method for preparing hericium erinaceus cultivation material through utilization of pecan production and processing waste

The invention provides a hericium erinaceus cultivation material. The hericium erinaceus cultivation material is characterized in that pecan branch scraps, outer shell scraps and shell scraps are used as main raw materials, cottonseed hulls, rice bran, bean cakes, calcium superphosphate, monopotassium phosphate, land plaster and the like are used as auxiliary materials, and the water content of the cultivation material is 63%-65%. The invention further provides a method for preparing the cultivation material. The hericium erinaceus cultivation material and the method have the advantages that the pecan branch scraps, the outer shell scraps and the shell scraps undergo sun exposure and secondary fermentation or piled ageing treatment, poisonous bacteriostat is removed, macromolecular substances are decomposed, and therefore the decomposed substances can be absorbed by hericium erinaceus hyphae easily; the cultivation material is reasonable in proportion and appropriate in PH, the hericium erinaceus hyphae are dense in growth, fruiting bodies are good in growth, and the biological efficiency reaches 123.5%-135.1%; a solution to innocent treatment of pecan branches, outer shells and shells is provided, and a novel matrix for hericium erinaceus cultivation is further found out.
Owner:邬方成

Preparation method for lithium-rich manganese based anode material hydroxide precursor

The invention discloses a preparation method for a lithium-rich manganese based anode material hydroxide precursor. The method includes the steps of: (1) preparing a mixed solution of a nickel salt, a cobalt salt and a manganese salt according to the mole ratio of Mn, Co and Ni in the hydroxide precursor's molecular formula MnxCoyNi1-x-y(OH)2, wherein x is greater than 0.5 and smaller than 1, y is greater than 0 and smaller than 0.5, and x+y is smaller than 1; (2) preparing an additive containing alkaline aqueous solution, and preparing a composite complexing agent solution containing EDTA, chitosan and ammonia water; (3) under inert gas protection, merging the mixed solution of the nickel salt, the cobalt salt and the manganese salt, the alkaline aqueous solution and the composite complexing agent solution and injecting the mixture into a continuous reaction kettle to carry out continuous reaction, controlling the average concentration of EDTA, chitosan and ammonia ions in the reaction solution, and controlling the reaction pH value at 9-13, the reaction temperature at 30-80DEG C and the stirring speed at 100-2000rpm; and (4) filtering, washing and drying the liquid naturally discharged from the reaction kettle. The lithium-rich manganese based anode material hydroxide precursor prepared by the method provided by the invention has the characteristics of uniform components, controllable particle size and compact growth.
Owner:有研科技集团有限公司

Method for making dwarf banana plants short and strong

The invention provides a method for making dwarf banana plants short and strong. The technological method comprises the steps that when field planting is completed in spring and cauloids of the dwarf banana plants are 1.0-1.3 meters high, paclobutrazol is applied to each dwarf banana plant, wherein 0.3-0.5 gram of paclobutrazol is mixed with 500-1000 milliliters of water, then the mixture of the paclobutrazol and the water is sprayed to the heads or the intersection portions of petiole base portions and the base portions of the cauloids of the dwarf banana plants, and then the dwarf banana plants grow for one month in the natural environment; then the leaf distance is obviously increased, and the paclobutrazol is applied to each dwarf banana plant for the second time, wherein 0.5-1.0 gram of paclobutrazol is mixed with 500-1000 milliliters of water, the mixture is sprayed to the heads or the intersection portions of the petiole base portions and the base portions of the cauloids of the dwarf banana plants, and the dwarf banana plants grow in the natural environment for one month; then the leaf distance is obviously increased again and the paclobutrazol is applied to each dwarf banana plant for the third time, wherein 1.0-2.0 grams of paclobutrazol is mixed with 500-1000 milliliters of water, and the mixture is sprayed to the heads or the intersection portions of the petiole base portions and the base portions of the cauloids of the dwarf banana plants. According to the method for making the dwarf banana plants short and strong, the wind resistance of the dwarf banana plants is improved, the dwarf banana plants are convenient to manage, and the yield and the quality of the dwarf banana plants are not influenced.
Owner:POMOLOGY RES INST GUANGDONG ACADEMY OF AGRI SCI

Preparation method of 3D printing material

The invention discloses a preparation method of a 3D printing material. The preparation method comprises the steps of extracting cobalt chloride and nickel chloride into an organic extraction agent, and compounding metatungstic acid into a solution; after the extraction agent containing cobalt and nickel and the metatungstic acid solution enter a mist spray chamber for a reaction in the form of mist spray, pouring out all materials in the mist spray chamber, and conducting filtration through a centrifugal machine; after a solid is washed, adding a glucose solution for slurrying; conducting mist spray drying, putting dried materials into a high-temperature furnace for calcination, and meanwhile, introducing inertia atmosphere, wherein the calcination portion is divided into three temperature areas; lowering the temperature till the temperature of the materials ranges from 25 DEG C to 30 DEG C; pouring the materials obtained after temperature reduction into a storage tank full of nitrogen; and then, conducting crushing through a nitrogen-protected airflow crusher, so that the 3D printing material is obtained. The preparation method of the 3D printing material is simple in process; and the 3D printing material which is high in apparent density, narrow in size distribution and high in hardness and strength can be obtained.
Owner:SHENZHEN POLYTECHNIC

Preparation method of friction-reduction anti-adhesion nano organic film based on micro device

The invention discloses a preparation method of a friction-reduction anti-adhesion nano organic film based on a micro device, comprising the following steps of: with aluminum, copper, magnesium and alloys thereof used in a micro/nano electromechanical system as substrate materials, matching different substrate materials selected from different water-soluble triazine organic compound salts with alkaline-support electrolysis salts; and preparing the nano organic film with hydrophobic function, friction reduction and adhesion resistance by adopting a three-electrode mode constant-current, cyclic-voltammetry and constant-potential organic film plating technology. A static contact angle of the prepared nano organic film and distilled water can reach above 110 degrees, a friction coefficient can be reduced below 0.05, the maximum adhesive force can be reduced to 103mN, the friction coefficient and the adhesive force can be effectively reduced, and the film thickness is controllable. The invention has the advantages of simple process, short period and low cost and easy industrialized production and can be widely used for the friction reduction and adhesion resistance of the micro device in the micro/nano electromechanical system and improve tribological characteristics.
Owner:SOUTH CHINA UNIV OF TECH

Preparation method for 2D/2D nitrogen-doped lanthanum titanate/sulfur-indium-zinc heterojunction photocatalyst

ActiveCN111085234AGood connection dispersionSolve the reunion puzzlePhysical/chemical process catalystsHydrogen productionHeterojunctionPhotocatalytic water splitting
The invention belongs to the technical field of industrial catalysis, and mainly discloses a preparation method for a 2D/2D nitrogen-doped lanthanum titanate/sulfur-indium-zinc heterojunction photocatalyst and an application of the 2D/2D nitrogen-doped lanthanum titanate/sulfur-indium-zinc heterojunction photocatalyst in hydrogen production by photocatalytic decomposition of water under full-lightirradiation. According to the invention, with a nitrogen-doped lanthanum titanate (N-La2Ti2O7) nanosheet as a substrate and polyfunctional trisodium citrate as a surfactant, the ZnIn2S4 nanosheet uniformly grows on the surface of the N-La2Ti2O7 nanosheet under a hydrothermal treatment condition, and a tight contact surface veneering type II-type heterojunction structure is formed between the ZnIn2S4 nanosheet and the N-La2Ti2O7 nanosheet, so the key problem of easy compounding of electron-hole pairs in a photocatalytic reaction process is well solved. The photocatalytic efficiency, the photo-induced electron migration path and the reaction mechanism of the catalyst are further determined through characterization of a photocatalytic water splitting hydrogen production activity test, a scanning electron microscope, a transmission electron microscope, ultraviolet-visible diffuse reflection, a PL fluorescence spectrum and the like. The series of catalysts are simple in preparation process, low in raw material cost, high in activity and applicable to large-scale production and practical application.
Owner:XI AN JIAOTONG UNIV
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