The application discloses a preparation method of hydroxyl nano-aluminum
oxide with controllable hydroxyl content, and relates to the technical field of inorganic functional material preparation. The method comprises the following steps: performing online gasification purification of an organic aluminum precursor in a closed integrated
reaction system; guiding the online gasification purified organic aluminum precursor into a
hydrolysis-hydrothermal
crystallization reaction zone through a
gas phase transportation channel, performing a controlled
hydrolysis reaction, and generating amorphous aluminum
hydroxide sol; sealing the
hydrolysis-hydrothermal
crystallization reaction zone, performing
hydrothermal treatment on the amorphous aluminum
hydroxide sol, and crystallizing the amorphous aluminum
hydroxide into hydroxyl nano-aluminum
oxide; and recovering and
drying the hydroxyl nano-aluminum
oxide. The application solves the fundamental contradiction between the improvement of material
chemical purity and the maintenance of surface functional hydroxyl in the prior art, avoids the damage of traditional
acid washing or
calcination to the hydroxyl, and significantly improves the dispersibility,
interface bonding force and
electrolyte wettability of the material in the field of
lithium ion batteries.