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61results about How to "Extensive research" patented technology

Test method of supercritical carbon dioxide content in coal

The invention discloses a test method of supercritical carbon dioxide content in coal. A determination device consisting of a vacuum pump, a coal sample tank, a carbon dioxide cylinder, a pressure device and a high-accuracy balance is used in the test method. The test method comprises the following steps of calculating the quantity of gas filled into an adsorption tank by measuring the mass variation of the adsorption tank, substracting the gas phase content increased in a free space of the adsorption tank to obtain the excess adsorption quantity of a coal sample under balance pressure, and calculating the gas phase carbon dioxide content in a coal pore by utilizing a non-ideal gas equation according to the pore pressure. The supercritical carbon dioxide content in coal is a sum of the excess adsorption quantity and the gas phase content of the pore space in coal, tests of a plurality of balance pressures can be finished by measuring carbon dioxide contents in the coal sample under different balance pressures. The test method has the advantages of simpleness and low requirement to an instrument and equipment, can accurately and conveniently measure the carbon dioxide content in coal and is beneficial to test research on the carbon dioxide content in coal.
Owner:CHINA UNIV OF MINING & TECH

Cantilever-beam electromagnetic-frictional-piezoelectric composite vibration energy harvester

The invention discloses a cantilever-beam electromagnetic-frictional-piezoelectric composite vibration energy harvester, and the energy harvester comprises a structural substrate fixed with an external excitation source, wherein the top of the structural substrate is connected with one end of a support beam elastic substrate. The top of one end of the support beam elastic substrate is movably connected with a cantilever beam elastic substrate, and the top of the other end of the support beam elastic substrate is sequentially provided with a frictional buffering layer and an electrode layer. The bottom of the other end of the support beam elastic substrate is provided with an electromagnetic induction coil, and the top of the other end of the cantilever beam elastic substrate is provided with a magnet. The bottom of the other end of the cantilever beam elastic substrate is provided with a frictional buffering layer, an electrode layer and a silica gel film layer, and the top of the cantilever beam elastic substrate is provided with a piezoelectric component. The energy harvester solves a problem that a conventional vibration energy harvesting device has a specific inherent frequency, and is low in energy utilization rate when the external excitation deflects from the specific inherent frequency.
Owner:XINZHOU TEACHERS UNIV

Circulating pipe network water quality comprehensive simulation test system with multi-channel flow switching calibration

The invention discloses a circulating pipe network water quality integrative simulation test system with multichannel flow switching and calibrating devices. The system comprises a water supply subsystem and an independent circulating pipe network subsystem, wherein the water supply subsystem comprises a first water supply water tank and a second water supply water tank; the first water supply water tank is provided with a water inlet, a water outlet and a chemical filling hole; the second water supply water tank is communicated with the first water supply water tank by a pipeline with a second valve and is provided with a water inlet, a water outlet and a chemical filling hole; the independent circulating pipe network subsystem is a loop comprising a main circulating pump, a multichannelflow switching and calibrating device and a high-level water replenishing and exhausting water tank which are connected in series by virtue of pipelines; the loop is connected with a first pipeline branch for realizing closed circulation, a water replenishing system, an emptying branch, a water quality online monitoring system and a temperature control system; and meanwhile, chemical filling systems are also connected on the pipeline of the independent circulating pipe network subsystem. All the components of the system cooperate with each other and the system has the advantages of high simulation degree and capability of simulating various working conditions of municipal water supply pipe network systems.
Owner:ZHEJIANG UNIV

A comprehensive water quality simulation test system for circulating pipe networks with visible pipe sections

The invention discloses a circulating pipe network water quality integrative simulation test system with visible pipe sections. The system comprises a water supply subsystem and independent circulating pipe network subsystems, wherein the water supply subsystem comprises a first water supply water tank and a second water supply water tank; the first water supply water tank is provided with a water inlet, a water outlet and a chemical filling hole; the second water supply water tank is communicated with the first water supply water tank by a pipeline with a second valve and is provided with a water inlet, a water outlet and a chemical filling hole; each independent circulating pipe network subsystem is a loop comprising a main circulating pump, a multichannel flow switching and calibratingdevice, a visible pipe section and a high-level water replenishing and exhausting water tank which are connected in series by virtue of pipelines; the loop is connected with a first pipeline branch for realizing closed circulation, a water replenishing system, an emptying branch, a water quality online monitoring system and a temperature control system; and meanwhile, chemical filling systems arealso connected on the pipeline of the independent circulating pipe network subsystem. All the components of the system cooperate with each other and the system has the advantages of high simulation degree and capability of simulating various working conditions of municipal water supply pipe network systems.
Owner:ZHEJIANG UNIV +1

Organic luminous material and preparation method thereof

The invention provides an organic luminous material and a preparation method thereof, and relates to an organic silicon polymer. Raw materials of the organic luminous material comprise metallic organic substance and polycarbosilane. The preparation method comprises the following steps of: putting polydimethylsiloxane into a reaction kettle, heating the polydimethylsiloxane under the protection ofargon, inflating the argon to the reaction kettle, adding n-hexane into the reaction kettle to dissolve the product after the temperature in the reaction kettle is naturally cooled to room temperature, filtering the product, removing the n-hexane in vacuum to obtain the polycarbosilane, soaking the ground polycarbosilane into ethanol, flushing the insoluble substances by using the ethanol and then drying the insoluble substances in vacuum; and pouring the polycarbosilane powder and the metallic organic substance powder into a three-necked bottle, heating the mixed powder to between 150 and 160 DEG C under the protective atmosphere of argon, preserving the heat for 1 to 1.5 hours, heating the mixed powder to between 260 and 270 DEG C, preserving the heat for 1 to 1.5 hours, dissolving the product by using the dry n-hexane after the reaction is finished and the product is cooled, filtering the product to remove the insoluble substances, and finally distilling the product with reduced pressure to obtain the powdery solid organic luminous material.
Owner:XIAMEN UNIV

Preparation technology for copper/graphite core-shell structure

The invention discloses a preparation technology for a copper / graphite core-shell structure. According to the technical scheme, RF-PECVD equipment is adopted, a copper film prepared through DPS-III type ultrahigh vacuum facing-target magnetron sputtering is used as a copper source, and a copper / graphite core-shell structure (GS / CC) material is successfully prepared. The preparation technology has the advantages that the copper / graphite core-shell structure material is prepared through direct-current magnetron sputtering and radio frequency plasma enhanced chemical vapor deposition methods. The field emission performance of the material can be effectively improved as Cu particles are introduced, the field emission performance of grapheme can be effectively improved by modulating the morphology of the grapheme, and therefore the material has potential application in a field emission device. By using complementary advantages of graphite and copper, the copper / graphite core-shell structure (GS / CC) material is prepared, while cost is reduced, the field emission performance of the core-shell structure material is promoted substantially, and the material has potential application in the fields of the information technology, biomedical science, sensors and the like.
Owner:QINGDAO SHENGLI BOILER

A comprehensive simulation test system for water quality of circulating pipe network with temperature control system

The invention discloses a circulating pipe network water quantity integrated simulation test system with a temperature control system. The system comprises a water supply subsystem and an independent circulating pipe network subsystem; the water supply subsystem comprises a first water supply tank and a second water supply tank, wherein the first water supply tank is provided with a water inlet, a water outlet and an agent injection port, and the second water supply tank is communicated with the first water supply tank by using a pipeline with a second valve and provided with a water inlet, awater outlet and an agent injection port; the independent circulating pipe network subsystem is a loop comprising a main circulating pump, an electromagnetic flow meter and a high-level water supply and exhaust water tank connected in series through a pipeline; and the loop is connected with a first pipeline branch for realizing closed circulation, a water supply system, an emptying branch, a water quality monitoring system and the temperature control system. The pipeline of the independent circulating pipe network subsystem is connected with an agent injection system. The circulating pipe network water quantity integrated simulation test system with the temperature control system has the advantages of high simulation degree and capability of simulating multiple actual municipal water supply pipe network system working conditions by cooperation of the components.
Owner:ZHEJIANG UNIV +1

A comprehensive water quality simulation test system for a circulating pipe network with a replacement pipe section

The invention discloses a water quality comprehensive simulation test system with replacement pipe sections for a circulating pipe network. The system comprises a water supply subsystem and independent circulating pipe network subsystems. The water supply subsystem includes a first water supply tank and a second water supply tank communicated with the first water supply tank through a pipeline with a second valve. Each independent circulating pipe network subsystem includes a main circulating pump, a multichannel flow switch calibration device, a visible pipe section and a loop of a high water supplement and exhaust tank that are connected in series by a pipeline. The loop is in connection with a first pipeline branch for realizing closed circulation, a water supplement system, a blowdownbranch, a water quality on-line monitoring system, a temperature control system and replacement pipe section branches. Meanwhile, the pipeline of the independent circulating pipe network subsystem isalso connected to a reagent filling system. Making use of the interaction among all parts, the water quality comprehensive simulation test system for a circulating pipe network has the advantages of high simulation degree and ability to simulate the working conditions of a plurality of municipal water supply pipe networks.
Owner:ZHEJIANG UNIV

Method for preparing nonenzymatic biosensor based on microelectrode array

The invention discloses a preparation method for preparing a microelectrode array based on a photoetching technology and preparing an electrochemical nonenzymatic biosensor by modifying the microelectrode array with a conductive element and an inorganic sensing coating layer, and relates to the field of macromolecular material science, photoetching technologies, electrochemical sensors and the like. Photoresist adopted in the preparation method can realize preparation of the microelectrode array with ultrahigh length-diameter ratio; a three-dimensional structure is developed on the basis of atwo-dimensional planar structure, so that the specific surface area of the coating layer is greatly enlarged, and a foundation is laid for the preparation of a high-sensitivity electrochemical sensor;meanwhile, the three-dimensional microarray structure improves the coarseness of the surface of the coating layer, and the effective load of a sensing coating layer is facilitated. A method for in-situ electrochemical reduction of inorganic transitional metal nano particles in the invention realizes preparation of an inorganic sensing coating layer having an electrochemical response, and has a synergistic effect together with a conductive microelectrode array. The technology disclosed by the invention is easy and convenient to operate; the constructed sensor has the advantages of high sensitivity to an object to be analyzed, high stability and the like.
Owner:JIANGNAN UNIV

High-temperature-resistant fiber filtering material for purifying industrial flue gas

The invention discloses a high-temperature-resistant fiber filtering material for purifying industrial flue gas, and belongs to the technical field of air purification. The fiber filtering material contains a dust facing surface fiber layer, a base cloth layer and a gas purifying surface fiber layer, wherein the dust facing surface fiber layer is made from composite fiber filtering materials which are prepared through the step of performing mixing, extruding and granulation on modified nano sepiolite, polyphenylene sulfide slices and a high-temperature antioxidant P-EPQ through a twin screw extruder, and PTFE emulsion coats the surfaces of the composite fiber filtering materials by a foam coating method, so that the diameters of filtering holes can be effectively reduced; the base cloth layer is made from fine polyphenylene sulfide fibers; and the gas purifying surface fiber layer is made from coarse polyphenylene sulfide fibers, so that the filtering resistance is not influenced, and the product abrasion resistance improved. According to the high-temperature-resistant fiber filtering material disclosed by the invention, the fact that sepiolite which is low in price is used for the flue gas filtering materials is a new breakthrough, besides, the purifying efficiency of industrial glue gas is improved, the dust removing times is reduced, the use temperature of the filtering materials is increased, and the service life is prolonged.
Owner:JIANGSU FUSHENG ENVIRONMENTAL PROTECTION GROUP

Chemical method for preparing halogenation methylamine lead photoelectric thin film in large-area manner

The invention relates to a chemical method for preparing a halogenation methylamine lead photoelectric thin film in a large-area manner. The method comprises the steps that a substrate deposited with a simple substance lead thin film and halogenation methylamine are heated under the vacuum or negative pressure condition, a reaction vessel is filled with halogenation methylamine, under the condition at the temperature of 200 DEG C to 300 DED C, the reaction is carried out, the reaction time is smaller than or equal to 50 min, and the halogenation methylamine lead semiconductor thin film material CH3NH3PbX3 with the large grain, good crystallinity and the uniform surface is prepared on the surface of the substrate material in an original manner, X is equal to Cl, Br, I or combination of one or two. According to the method, the halogenation methylamine lead thin film can be rapidly prepared in the large-area manner, the prepared halogenation methylamine lead thin film is good in thickness uniformity, halogenation methylamine lead is good in crystal and large in crystal size, the diameter can reach 0.5 to 2 micrometers, preferably, the diameter can reach one to three micrometers, the problem that in the traditional method, the film formation grain is small is solved, and the method has the wide experiment device research and industrial application prospect.
Owner:XUCHANG UNIV
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