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150results about How to "Moderate working conditions" patented technology

Method for extracting grease from oil-tea camellia seed kernel and recovering saponin and saccharide active substances

The invention discloses a method for extracting grease from oil-tea camellia seed kernel and recovering saponin and saccharide active substances, comprising the following steps of: (1) crushing and tempering: with hull-removed oil-tea camellia seed kernels as raw materials, crushing and grinding the materials, adding water for uniformly stirring, wherein the quality-volume ratio of the oil-tea camellia seed kernels to the water is 1kg:2-8L and controlling the temperature of the system to be 30-60DEG C; (2) carrying out the enzymolysis: adjusting the pH value of the system to be 3.5-8.0, adding pectinase the weight of which is 0.1-2 percent that of the camellia seed kernels and carrying out the enzymolysis for 2-5h; (3) heating and centrifuging: treating the system at the temperature of 80-90DEG C for 5-15min after enzymolysis; and (4) recovering the grease and the active substances: in which, the centrifuged and separated system comprises boiled oil, liquid phase and residue, taking out the boiled oil and spray-drying the liquid phase to obtain the active substances containing the saponin and saccharide. The method for extracting the grease avoids the high-temperature pretreatment of high-temperature enzymolysis of oil materials and can be used for synchronously recovering oil and a saponin and saccharide mixture which can be used as a saponin crude product or a feed additive.
Owner:ACAD OF NAT FOOD & STRATEGIC RESERVES ADMINISTRATION

Method for preparing fish-skin collagen powder by use of fresh fish skin

The invention relates to a method for preparing a fish-skin collagen powder by the use of fresh fish skin. The method comprises the following steps: fresh fish skin is selected as a raw material and is immersed in sodium hydroxide, the fresh skin is washed with water to neutral pH after fat and impure protein on the surface of the fish skin are removed, and crushing is carried out; drinking water and edible vinegar are added to the crushed fish skin and uniform agitation is carried out, ultrasonication and deodorization treatments are carried out, and papain is added to carry out controlled-enzymatic hydrolysis so as to obtain a fish-skin enzymatic hydrolysate; active carbon is added for decarburization clarification after enzyme deactivation, filtration is carried out, and a filtrate undergoes concentration and spray drying so as to obtain the fish-skin collagen powder. By ultrasonication of the fish skin, active ingredients in acetic acid are activated to react with fishy smell substances in the fish skin so as to remove the fishy smell. By adding active carbon into the enzymatic hydrolysate to carry out decarburization clarification for fishy smell elimination and decoloration, the prepared fish-skin collagen powder has no fishy smell. The method provided by the invention has advantages of advanced technology, reasonable process and controllable operation, and is suitable for large-scale production.
Owner:威海市桢昊生物技术有限公司

Cleaner production method for synthetizing chloromethane

The present invention discloses a cleaner production method for synthetizing chloromethane. The method comprises the steps: 1), synthetizing chloromethane: synthetizing crude chloromethane from gas-phase hydrogen chloride and gas-phase methanol; 2), recovering waste heat: performing heat exchange on the crude chloromethane by a heat exchange device and liquid methanol, cooling and discharging, wherein liquid methanol is heated by the heat exchange device to form gas-phase methanol which enters the step 1) as a raw material to react; 3), deacidifying by a deacidifying tower: deacidifying the crude chloromethane; 4), refining in an absorption tower; 5), pressurizing, extracting, rectifying and removing ether; and 6) performing diluted acid solution membrane concentration. In the method, the pressure application ranges of the hydrogen chloride and the methanol are relatively wide, and the content of HCl in diluted acid solution is greatly reduced; the methanol is used as a washing solution, other secondary wastes can not be generated; raw materials, such as the methanol and HCl, are utilized to the greatest extent; the unit energy consumption of CH3Cl is greatly reduced, the unit energy consumption of a product, namely CH3Cl is reduced by more than 20% compared with that in an industrialized unit in the prior art.
Owner:南通科恩化工技术有限公司

Preparation process of red date condensed juice high in cAMP content

The invention discloses a preparation process of red date condensed juice high in cAMP content. The preparation process includes the following steps of firstly, conducting separating, washing and smashing; secondly, conducting hot water extraction; thirdly, conducting cooling and heat preservation enzymic method oriented conversion; fourthly, adding composite enzyme preparations; fifthly, inactivating enzymes; sixthly, conducting centrifugation; seventhly, conducting filtration; eighthly, conducting concentration and pasteurization; ninthly, conducting filling. Compared with the prior art, the preparation process has the advantages that the process is simple, the production period is shortened, and the energy loss is reduced; extraction is conducted after smashing is conducted, and therefore extraction of nutritional ingredients in red dates can be improved; by means of the extraction and enzymolysis combined method, the juice yield is greatly improved, the processing time is greatly shortened, and the cyclic adenosine monophosphate content in red date juice is improved; date peel is utilized, and the cAMP content is improved; preparations of pectinase, cellulose and protease are used in a composite mode, and the hydrolysis capacity of enzymic preparations is improved; the step-by-step enzymolysis and extraction process is adopted, and interference between related enzyme preparations is avoided.
Owner:河北九维生物科技开发有限公司

Extraction method of effective components of Chinese angelica

The invention relates to an extraction method of effective components of Chinese angelica. The extraction method comprises the following steps: 1, Chinese angelica is crushed; 2, crushed Chinese angelica is added to a solvent A solution with the pH value of 5.5; 3, cellulase with the concentration of 0.3mg.mL<-1> is added to the solution obtained in step 2; 4, the solution obtained in step 3 is subjected to enzymatic hydrolysis for 6h at a constant temperature of 55DEG C; 5, isoamylase with the concentration of 0.3mg.ml<-1> is added to the solution obtained in step 4; 6, a solution obtained in step 5 is subjected to enzymatic hydrolysis for 6h at a constant temperature of 55DEG C; 7, the solution obtained in step 6 is subjected to reduced pressure filtration after completing the enzymatic hydrolysis, and the obtained filtrate is preserved in a dark place; 8, the filter residue obtained by filtering in step 7 is used for extracting ligustilide, an eight time solvent B is added each time, reflux extraction is twice carried out for 2h, the obtained first filtrate and the obtained second filtrate are mixed to obtain a mixed filtrate which is a ligustilide solution, and the ligustilide solution is preserved in a low temperature dark place; 9, the filter residue obtained in step 8 is used for extracting angelica polysaccharides, an fifteen time solvent C is added to the filter residue to extract; 10, the filtrate obtained in step 9 is concentrated to obtain a concentrate; and 11, a solvent D is added to the concentrate obtained in step 10 until that the concentration of the solvent D reaches 75% to obtain a deposition, and the deposition is centrifuged by a centrifuge to obtain the angelica polysaccharides.
Owner:LANZHOU UNIVERSITY OF TECHNOLOGY
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