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91results about How to "Facilitate blending" patented technology

Water-borne woodware coating containing modified polyurethane emulsion and preparation method thereof

The invention provides a water-borne woodware coating containing a modified polyurethane emulsion and a preparation method thereof. The water-borne woodware coating is composed of the following components: water, a thickening agent, a defoaming agent, a pH regulator, an antifreezing agent, a film-forming auxiliary agent, the modified polyurethane emulsion, a levelling agent, a nano inorganic antibacterial aldehyde removing agent, and water-borne paint inorganic hardening resin. The selected modified polyurethane emulsion includes a self-crosslinkable polyurethane acrylate composite emulsion, a core-shell interpenetrated network-structure polyurethane acrylate copolymer emulsion, a silane coupling agent modified polyurethane acrylate composite emulsion, and an epoxy resin modified polyurethane emulsion. The plurality of emulsions are added to the water-borne woodware paint, and thus the coating has the properties of high hardness and adhesion force, and good water resistance, alcohol resistance and pollution resistance; the selected nano inorganic antibacterial aldehyde removing agent has the effects of environmental protection, safety, no toxicity, and long-term bacterial resistance; and the selected water-borne inorganic hardening resin is used for improving the hardness, the adhesion force and the chemical resistance of the water-borne paint.
Owner:SKSHU PAINT

Low-temperature toughened and reinforced PC/PBT (polycarbonate/polybenzothiazole) alloy material and preparation method thereof

The invention relates to a low-temperature toughened and reinforced PC/PBT (polycarbonate/polybenzothiazole) alloy material and a preparation method thereof. The PC/PBT alloy material is prepared from raw materials such as PC resin, PBT, a low-temperature toughening agent, a reinforcing agent, a bulking agent and an antioxidant, wherein the toughening agent is diolefin-styrene-methyl methacrylate (MBS/MIS) which is of a core-shell structure, the reinforcing agent is non-alkali chopped glass fiber, the bulking agent is an ethylene-methyl acrylate copolymer (EMA), and the antioxidant is prepared by compounding an antioxidant 1010 and an antioxidant 168. The preparation process disclosed by the invention is implemented by using single and double screw extruders in cooperation with a two-step extrusion process, the technical characteristic is stepwise feeding, and the preset temperatures of the two extruders are differentiated. Through the implementation of the formula and the process, a low-temperature-resistant and high-strength PC/PBT alloy material which is excellent in performance and good in appearance can be prepared, and the PC/PBT alloy material can be widely used in the aspects of auto parts, bumpers, elevator parts, electrical and electronic engineering, engineering assembly parts for cold regions, and the like.
Owner:SHAANXI RES DESIGN INST OF PETROLEUM CHEM IND

Rice-husk-based carbon/silicon composite used as rubber filler and preparation method thereof

The invention discloses a rice-husk-based carbon/silicon composite used as a rubber filler and a preparation method thereof, and belongs to the technical field of the preparation of carbon/silicon fillers. The method comprises the following steps of: pre-carbonizing a raw material, namely rice husks in a muffle furnace at low temperature so as to remove the moisture and volatile substances from the rice husks, carbonizing in a vacuum sintering furnace, and controlling sintering conditions to obtain a rice-husk-based carbon/silicon composite with high silicon content, wherein the carbon accounts for 65 to 75 percent of the total weight of the carbon/silicon composite, the nitrogen adsorption Brunauer-Emmett-Teller (BET) specific surface area is 12 to 75m<2>/g, and the dibutyl phthalate (DBP) absorption number is 1.7 to 3.8cm<3>/g; and treating the rice-husk-based carbon/silicon composite with high silicon content by using solution of sodium hydroxide or potassium hydroxide, and dissolving out most of silicon dioxide to obtain the rice-husk-based carbon/silicon composite with low silicon content, wherein the carbon accounts for 85 to 98 percent of the total weight of the rice-husk-based carbon/silicon composite, the specific surface area is 120 to 196 m<2>/g, and the DBP absorption number is 2.1 to 3.0cm<3>/g. The rice-husk-based carbon/silicon composite serving as a reinforcingagent and a filler is widely applicable to various models of rubber varieties; moreover, the rice-husk-based carbon/silicon composite is an excellent dual phase filler.
Owner:JIANGNAN UNIV

Olefin copolymer with polar monomer structural units and preparation method of olefin copolymer

ActiveCN104558347AHas a melting pointHigh melting pointPolymer scienceAlpha-olefin
The invention relates to an olefin copolymer with polar monomer structural units and a preparation method of the olefin copolymer with the polar monomer structural units. The olefin copolymer is prepared from polar monomers, a monomer 4-methyl-1-pentene and other monomers through copolymerization. The general formula of the olefin copolymer is as shown in the description, wherein n, m and p respectively represent number-average degrees of polymerization of the monomer 4-methyl-1-pentene, the polar monomers and the other monomers in the copolymer, and the monomer structural units are randomly distributed in the sequence and are isotactically distributed in a stereoscopic structure. By introducing polar monomer structural units in a polymer chain, the surface performance of the polymer can be effectively improved when a high melting point is maintained, and the surface energy is improved. The preparation method comprises the step of carrying out copolymerization on the polar monomers, the monomer 4-methyl-1-pentene and the other monomers by virtue of a polymerization catalyst system, so as to prepare the olefin copolymer with the polar monomer structural units, wherein the polymerization catalyst system is capable of polymerizing alpha-olefin into an isotactic polymer and contains transition metal compounds.
Owner:CHINA PETROLEUM & CHEM CORP +1

Grade-1E K2-type radiation cross-linked halogen-free flame-retardant cable material for nuclear power plant and preparation method thereof

The invention relates to a grade-1E K2-type radiation cross-linked halogen-free flame-retardant cable material for a nuclear power plant and a preparation method thereof, belonging to the field of new chemical materials. The cable material comprises raw materials including base resin EVA (ethylene-vinyl acetate copolymer), flame retardants A and B, a flame retardant synergist, basic antioxidants 1010 and 168, a radiation-resistant auxiliary agent 4,4'-thiobis(6-tertiary-butyl-3-methylphenol) and a processing agent; and the preparation method comprises the process steps of material weighing, pretreatment, mixing, extrusion granulation, drying and the like. The cable material is a red-phosphorus-free halogen-free environment-friendly flame-retardant material, phenoxy polyphosphazene is used as a main flame retardant in a flame-retardant system of the cable material, an inorganic flame retardant is auxiliary, the flame-retardant system accounts for a small weight percentage of the material, and the cable material is high in flame-retardant efficiency and excellent in mechanical properties, processability and radiation resistance, so that the cable material is a novel environment-friendly flame-retardant material which has excellent comprehensive properties and is suitable for a nuclear power plant environment.
Owner:SICHUAN INST OF ATOMIC ENERGY +1

Preparation method of radiation-resistant organic silicon packaging adhesives

The invention provides a preparation method of radiation-resistant organic silicon packaging adhesives. The method includes the following steps that (1) a titanate coupling agent is dispersed in an n-butanol aqueous solution with the mass fraction being 80%, modified liquid is obtained after room-temperature stirring, nano cerium oxide is added into the modified liquid for magnetic stirring, pressure reduction and rotary evaporation are carried out on the mixture after reflux condensation, the mixture is dried till the weight is constant, the mixture is obtained and ground, and accordingly modified nano cerium oxide is obtained; (2) by mass, poly (methyl phenyl siloxane), PEEK, ethyl methacrylate and the modified nano cerium oxide obtained in the step (1) are added into an internal mixer for mixing, the mixture is moved into a single-screw extruding machine to be melted and extruded, and a granular material is obtained after cooling and granulation; (3) by weight, a cross-linking agent, a tackifier and the particle material obtained in the step (2) are added into a high mixing machine for high-speed mixing, high-speed mixing continuous being carried out after an inhibitor is added, medium-speed mixing is carried out after a catalyst is added, and the radiation-resistant organic silicon packaging adhesives are obtained after discharging. The organic silicon packaging adhesives prepared through the method are good in radiation resistance.
Owner:DONGGUAN XINXING ORGANIC SILICON TECH

Organic-inorganic hybrid membrane for pervaporation separation of methanol/methyl acetate azeotropic system and preparation method thereof

The invention discloses an organic-inorganic hydrid film used for pervaporation separation of a methanol / methyl acetate azeotropic system and a preparation method thereof. The preparation method comprises the following processes of: (1) heating and stirring polyvinyl alcohol (PVA), polyvinylpyrrolidone (PVP), a 4A molecular sieve and a solvent of dimethyl sulfoxide according to proportions in a constant-temperature water bath to obtain a PVA / PVP / 4A molecular sieve mixing solution; and (2) weighing DAS (Dialdehyde Starch) according to a proportion, dissolving into the dimethyl sulfoxide, stirring in a dark place and dissolving, then adding the equivalent PVA / PVP / 4A molecular sieve mixing solution obtained in the step (1) to the solution, and uniformly stirring to obtain a casting film solution. The casting film solution is filtered and defoamed, and then the film is scraped from glass and dried. The dried film is placed below a high-pressure mercury lamp and irradiated for 30-60 min toensure that coupling reaction is completed so as to obtain a 4A molecular sieve-filled DAS-crosslinking polyvinyl alcohol / polyvinylpyrrolidone organic-inorganic hydrid film. The organic-inorganic hydrid film has favorable mechanical strength and chemical stability and a higher pervaporation separation coefficient and can effectively break azeotropic components and has better separation degree than the traditional method.
Owner:NINGBO UNIV

Production technology of activation and oxidation double-modified scrap tire rubber powder modified asphalt

The invention discloses a production technology of activation and oxidation double-modified scrap tire rubber powder modified asphalt. According to the production technology, low temperature plasma activation is carried out on desulfurated scrap tire rubber powder, the obtained rubber powder is then sequentially treated by etching and surface oxidation, and the scrap tire rubber powder modified asphalt is prepared by adopting a wet process under the action of a high speed shearing machine. After the rubber powder is subjected to low temperature plasma activation, the specific surface area of the rubber powder is enlarged, so that the effective contact area between the rubber powder and asphalt is increased, and the rubber powder is promoted to be blended with the asphalt; on the other hand, oxygen containing functional groups can be introduced, the contents of -OH groups and C=C double bonds in the rubber powder are increased, and surface oxidation treatment is then carried out, so that the content of active groups on the surface of the rubber powder is further increased, the compatibility of the rubber powder and the asphalt is improved, the softening point of the modified asphalt is obviously increased, and the pavement performance of the modified asphalt is greatly improved.
Owner:安徽中宏橡塑有限公司

High-efficiency oxygen-insulation water-insulation blended full-degradable plastic film and preparation method thereof

The invention discloses a high-efficiency oxygen-insulation water-insulation blended full-degradable plastic film. The high-efficiency oxygen-insulation water-insulation blended full-degradable plastic film is prepared from, by weight, 60 to 65 parts of corn starch, 7 to 9 parts of nano montmorillonite, 0.6 to 0.7 part of peanut oil, 1.2 to 1.4 parts of tetrabutyl titanate, 12 to 14 parts of ramie straw, 27 to 30 parts of polyvinyl alcohol, 1 to 2 parts of xanthan gum, 2 to 4 parts of sodium carboxymethylcellulose, 14 to 15 parts of polyethylene glycol, 7 to 9 parts of poly propylene carbonate, 4 to 6 parts of Pulullan, and 2 to 3 parts of ethyl silicon oil. According to a preparation method, synergistic effect of polyving akohol, polyethylene glycol, and poly propylene carbonate is realized; so that the melting point of polyving akohol is reduced, better blending with a starch master batch is realized, barrier property of plastic film is improved, and oxygen insulation and water insulation effects are excellent. The high-efficiency oxygen-insulation water-insulation blended full-degradable plastic film can be taken as food packaging bags and preservative film, and is capable of insulating oxygen and water, and realizing fresh-keeping effects; and prepared products are capable of satisfying using requirements and can be degraded rapidly after abandoning.
Owner:TONGLING FOUNDER PLASTICS TECH

Preparation method of antimony doped nanometer stannic oxide powder

The invention discloses a preparation method of an antimony doped nanometer stannic oxide powder. The preparation method comprises the following steps: (1) mixing an antimonic salt and a tin salt, dissolving in an ethyl alcohol solution, and conducting ultrasonic concussion for 10-20 minutes at the room temperature to obtain a solution A; sequentially dissolving butanetetracarboxylic acid and ammonium dihydrogen phosphate into deionized water to obtain a solution B; (2) mixing the solution A and the solution B, conducting ultrasonic concussion for 5-10 minutes at the room temperature, adding alkali and diethanol amine at the stirring state, enabling the pH of the solution to reach 8-9, heating to 65-75 DEG C, reacting for 2-4 hours to obtain a precipitate precursor; and (3) washing, dryingand calcining the precipitate precursor to obtain the antimony doped nanometer stannic oxide powder. The prepared antimony doped nanometer stannic oxide powder is even in particle size distribution and good in dispersity, the average particle size of the prepared antimony doped nanometer stannic oxide powder is less than 120 nm, the electrical resistivity is less than 25 ohm.cm, the specific surface area is 4-6 m<2>/g, and the electrical conductivity is excellent.
Owner:广西生富锑业科技股份有限公司

Polymer quaternary phosphonium salt antibacterial material and preparation method thereof

The invention discloses a high polymer quaternary phosphonium salt antibacterial material and a preparation method thereof. The high polymer quaternary phosphonium salt antibacterial material is prepared by bonding halogenacylhalide type monomers onto macromolecules of an ethylene-vinyl alcohol copolymer (EVOH) through grafting reaction and further performing quaternary phosphonium reaction with trialkylphosphine. The high polymer quaternary phosphonium salt antibacterial material disclosed by the invention has the advantages of broad-spectrum, high-efficient and lasting antibacterial function and good safety, can be shaped and processed into products with the antibacterial function alone, and mixed with polyethylene, polypropylene and other non-polar resin and other types of resin for being shaped and processed into the products with the antibacterial function, and further has broad application prospects. The sterilization efficiency of the high polymer quaternary phosphonium salt antibacterial material prepared by the preparation method disclosed by the invention against escherichia coli, staphylococcus aureus and a variety of bacteria is more than 99%, and the mildew-resistant grade against aspergillus niger, aspergillus terreus and a variety of mildew is 1-0 grade.
Owner:JINYU HENAN PACKAGING

Waterborne wood paint containing modified polyurethane emulsion and preparation method of waterborne wood paint

The invention provides waterborne wood paint containing modified polyurethane emulsion and a preparation method of the waterborne wood paint. The waterborne wood paint containing the modified polyurethane emulsion is prepared from the following components: water, a thickener, a de-foaming agent, a pH (Potential of Hydrogen) regulator, an anti-freezing agent, a film-forming auxiliary agent, the modified polyurethane emulsion, a flatting agent, a nano inorganic antibacterial formaldehyde removing agent and waterborne paint inorganic hardening resin, wherein the selected modified polyurethane emulsion is prepared from self-cross-linked polyurethane acrylate composite emulsion, polyurethane acrylate copolymerized emulsion with a core-shell interpenetrating network structure, silane coupling agent modified polyurethane acrylate composite emulsion and epoxy resin modified polyurethane emulsion. The emulsions are added into the waterborne wood paint, so that the waterborne wood paint has very high rigidity and adhesive force and good water resistance, alcohol resistance and pollution resistance; the nano inorganic antibacterial formaldehyde removing agent is selected, so that the waterborne wood paint has environment-friendly, safe and toxin-free, and long-period antibacterial effects. The waterborne paint inorganic hardening resin is used for improving the rigidity, adhesive force and chemical resistance properties of the waterborne paint.
Owner:SKSHU PAINT

Copper-aluminum-manganese alloy/ polymer/ carbon nanotube damping material and preparation method

ActiveCN109277571AReduce the proportionPrecise control of hole structure parametersMaterials preparationEnergy absorption
The invention discloses a copper-aluminum-manganese alloy / polymer / carbon nanotube damping material and a preparation method and belongs to the technical field of damping material preparation. The damping material comprises a porous copper-aluminum-manganese memory alloy framework and a thermoplastic elastomer. The thermoplastic elastomer is acquired by blending polyacrylate rubber, polyvinyl chloride and carbon nanotubes together. The thermoplastic elastomer is loaded in pores of the copper-aluminum-manganese memory alloy framework. The pore diameter of the porous copper-aluminum-manganese memory alloy framework ranges between 0.355 Mu m and 1.43 Mu m, and the pore rate of the porous copper-aluminum-manganese memory alloy framework ranges between 70% and 90%. The porous copper-aluminum-manganese shape memory alloy with high anti-martensite stabilization capacity and with pores communicating with each other is adopted as the framework. The thermoplastic elastomer generated by a polyacrylate composite material (ACM) polymer, a polyvinyl chloride (PVC) polymer and carbon nanotubes (CNT) is infiltrated into the communicating pores. According to the composite material, the proportionof the damping alloy can be effectively reduced; and disadvantages of the polymer damping material that the strength is not enough and dimensional stability is poor can also be remedied. By adopting the porous copper-aluminum-manganese shape memory alloy framework, pore structure parameters can be controlled accurately; and in addition, the porous copper-aluminum-manganese shape memory alloy framework has the advantages of being great in energy absorption, high temperature resistance and good in dimensional stability.
Owner:CENT SOUTH UNIV
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