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69results about How to "Adjust ratio" patented technology

Co-production method for methyl benzoic acid and phthalic acid

The invention discloses a co-production method for methyl benzoic acid and phthalic acid. The co-production method comprises the following steps: (1) continuously introducing fresh dimethylbenzene, a catalyst and oxygen-containing gas into a primary oxidation reactor for a reaction to obtain a primary oxidation reaction solution containing methyl benzoic acid and an eight-carbon oxygen-contained compound; (2) carrying out continuous cooling, crystallization and filtration on the primary oxidation reaction solution to obtain filter liquor and filter cake, circulating 1-98% of the filter liquor back the primary oxidation reactor continuously, and continuous rectifying the filter cake continuously, to obtain a low-boiling point front cut fraction, distillation raffinate and a methyl benzoic acid product separately; (3) adding the remaining filter liquor in the step (2) and the obtained front cut fraction and distillation raffinate in the step (2) into a secondary oxidation reactor continuously, and meanwhile continuously introducing a Co/Mn/Br catalyst, acetic acid and oxygen-containing gas into the secondary oxidation reactor for an oxidation reaction to obtain a secondary oxidation reaction mixture; and (4) continuously cooling, crystallizing and filtrating the secondary oxidation reaction mixture to obtain a filter liquor and a phthalic acid product. The co-production method has advantages of a simple process, a low cost, a high yield, good selectivity, good economic benefits, and environmental protection.
Owner:山东友道化学有限公司

Double-temperature water-heating series two injection type concurrent control valve and manufacturing method thereof

A downstream control valve of two-pouring type of dual-temperature water heating series and a manufacture method thereof are provided. The invention includes a one-step forming valve body, a valve rod, a spiral handle, a valve cover, a valve core and a post forming valve body. The one-step forming valve body is formed in a first-time die by injection molding. A blank cap and a closure head are arranged on the one-step forming valve body and then the one-step forming valve body is placed in a second-time die chamber to form the post forming valve body which wraps the one-step forming valve body. The valve rod, the spiral handle and the valve cover are mounted on the forming valve body. The upper sheet of the valve core, the middle sheet of the valve core, the bottom sheet of the valve core and the cushion of the valve core are mounted in turn in the spool chamber of the forming valve body. In order to reduce the production cost of the prior water tap and improve the sanitary quality of the water, metal material is replaced by plastic and the through hole injection molding and the post forming technology are adopted. When the water tap is rotated left or right, the hot or the cold water can be provided. With the advantages of high sensitivity of temperature control and high service efficiency, the invention solves the problem of high cost for the prior water tap and has a broad market foreground.
Owner:赵雨欧

Dual-mode multi-beam electronic gun for dual-mode traveling wave tube and method for controlling dual-mode multi-beam electronic gun

The invention discloses a dual-mode multi-beam electronic gun for a dual-mode traveling wave tube and a method for controlling the dual-mode multi-beam electronic gun. The dual-mode multi-beam electronic gun comprises a cathode, a shade gate, an internal grid, an external grid and an anode, which are arranged in sequence, wherein the cathode comprises a cathode molybdenum tube, the inside of which is divided into two parts along the axis of the cathode molybdenum tube; the two parts are separated by insulating ceramic; a cathode sponge body is mounted in one part, and a filament filling and sealing insulator is mounted in the other part and is internally provided with a filament; the end face of the cathode molybdenum tube is provided with a plurality of holes; the internal grid controls the electronic beams in partial holes, and the external grid controls the electronic beams in the rest holes so as to implement dual-mode operation. According to the dual-mode multi-beam electronic gun and the method, a high-mode operation state and a low-mode operation state can be provided, and the control voltage is consistent, so that the electronic beams in two modes can be focused by the same magnetic field.
Owner:HUADONG PHOTOELECTRIC TECHN INST OF ANHUI PROVINCE

Nucleus pulposus-cartilage extracellular matrix scaffold and preparing method thereof

InactiveCN105031734AOvercome the disadvantages of small quantities and difficult accessGood biocompatibilityProsthesisArticular surfacesArticular surface
The invention discloses a nucleus pulposus-cartilage extracellular matrix scaffold and a preparing method thereof and belongs to the biological tissue engineering technology. The preparing method comprises the steps that nucleus pulposuses and bony articular surface cartilage are smashed, decellularized, subjected to gradient centrifugation to collect extracellular matrix microfilament suspension, and freeze-dried to obtain a freeze-dried decellularized nucleus pulposus matrix and a freeze-dried decellularized cartilage matrix, the two matrixes are taken in certain proportion and dissolved in ultrapure water to prepare mixed matrix suspension with certain concentration, and the mixed matrix suspension is freeze-dried and subjected to ultraviolet irradiation crosslinking and chemical reagent crosslinking in sequence so that the nucleus pulposus-cartilage extracellular matrix scaffold can be obtained. In this way, the defect that the nucleus pulposuses are hard to obtain due to the small number is overcome; the preparing technology is simple, and decellularizing can be achieved thoroughly; the matrix scaffold is degradable and high in biocompatibility; the matrix scaffold is of a three-dimensional structure, is high in mechanical property and plasticity, and can facilitate the distribution, growth and differentiation of seed cells; the freeze-dried extracellular matrixes are convenient to store and prepare and can be used for constructing a tissue engineered intervertebral disc to repair partial defects of the intervertebral disc, and broad clinical application prospects are realized.
Owner:TIANJIN HOSPITAL

Foamy copper in-situ growth copper oxide/cuprous oxide photocatalytic material as well as preparation method and application thereof

PendingCN113546624ARegulating absorbencyRegulating photocatalytic activityWater/sewage treatment by irradiationWater treatment compoundsElectrolytic agentNanoparticle
The invention discloses a foamy copper in-situ growth copper oxide/cuprous oxide photocatalytic material as well as a preparation method and application thereof. The preparation method comprises the following steps of dissolving NaOH in deionized water to obtain a solution A, adding NaCl into the solution A to obtain a solution B, and adding a dispersing agent into the solution B to obtain a solution C, taking a foam copper sheet as an anode, taking an inert electrode as a cathode, taking the solution C as electrolyte, enabling the anode to be subjected to oxidation treatment, then using deionized water for repeatedly washing the foam copper sheet subjected to anodic oxidation, and acquiring a product D attached with a black active substance, and annealing the product D to obtain the foamy copper in-situ growth copper oxide/cuprous oxide photocatalytic material. The phase-controllable copper oxide/cuprous oxide photocatalytic film material is obtained, the microtopography of the material is regulated and controlled from coexistence of nanorods and nanoparticles to regulation and control of the nanoparticles, and the light absorption and photocatalytic activity of the photocatalytic film are regulated and controlled by controlling the phase and the topography.
Owner:SHAANXI UNIV OF SCI & TECH

Muskmelon seedling growing substrate

The invention discloses a muskmelon seedling growing substrate, and belongs to the technical field of seedling growing substrates. The muskmelon seedling growing substrate is prepared from thoroughly-decomposed maize straw, thoroughly-decomposed chicken dung, turfy soil, vermiculite, antagonistic actinomycetes and chitosan, and the mass ratio of thoroughly-decomposed maize straw to thoroughly-decomposed chicken dung to turfy soil, vermiculite to antagonistic actinomycetes to chitosan is 1:(0.08-0.12):(0.8-1.2):(0.8-1.2):(0.04-0.06):(0.06-0.1). According to the muskmelon seedling growing substrate, the substrate contains antagonistic actinomycetes, the antagonistic actinomycetes has the good colonization capability in rhizosphere soil, the good inhibiting effect is achieved for greenhouse soil-borne diseases, and the continuous cropping obstacle can be effectively repaired; the PPO activity of muskmelon seedling stage leaves and roots is improved, and the muskmelon plant disease resistance is improved; the substrate is a compound substrate, the substrate is loose and good in water binding capacity, the total-P, total-K, quick-acting N, quick-acting P and quick-acting K contents arehigh, the fruit quality can be improved, and the fruit yield can be increased.
Owner:新疆生产建设兵团第十师科学技术局

Process for step-by-step improvement of methane conversion through methane cracking and carbon elimination

The invention provides a process for step-by-step improvement of methane conversion through methane cracking and carbon elimination. The process comprises the following steps: introducing mixed gas of CH4 and Ar into a fixed bed filled with a catalyst and carrying out a methane cracking reaction at a pressure of 0.1 to 3 MPa and a temperature of 300 to 900 DEG C for 10 to 60 min; carrying out purging with Ar; introducing carbon elimination gas and carrying out a carbon elimination reaction at a pressure of 0.1 to 3 MPa and a temperature of 400 to 900 DEG C for 15 to 60 min; carrying out purging with Ar again to finish a methane conversion reaction once; and repeating the cracking reaction and the carbon elimination reaction to complete the methane conversion reaction a plurality of times. According to the invention, the methane cracking reaction is carried out first and then the carbon elimination reaction is carried out so as to eliminate accumulated carbon the surface of a catalyst; since the separate two-step reactions need low temperature, energy consumption is reduced and sintering of the catalyst at high temperature is avoided at the same time; and the method allows the catalyst to maintain catalytic activity for a long time.
Owner:NORTHWEST UNIV

Ink separating device for rainbow printing

The invention discloses an ink separating device for rainbow printing. The ink separating device comprises two fixed rods which are arranged in parallel and distributed obliquely; two ends of the fixed rods are fixed to a support of a side plate of a printing machine; a plurality of threaded mounting holes are formed in the fixed rods, and a separating plate is mounted through screws; the separating plate is composed of a triangular plate with an arc side; an elastic cushion block of an arc-shaped structure is arranged at the arc side of the separating plate; one side of the separating plate is arranged against an inclined plate of the printing plate and while the other side of the separating plate is tightly ejected through the screws on the fixed rods; the arc side of the separating plate is arranged against an ink duct roller. According to the ink separating device for rainbow printing, one side of the separating plate is inclined against the inclined plate of the printing machine and while the other side of the separating plate is tightly ejected with the screws, thus reliable and firm positioning is realized; the separating plates can be simply dismounted by unscrewing the screws, and the operation is convenient and simple; in addition, the plurality of mounting holes are formed in the fixed rods, so that the installation position of the separating plate can be adjusted freely as requirement, and as a result, the ratio adjustment of each type of ink is realized; the ink separating device is simple in structure and easy to be operated.
Owner:WUXI DOUBLE DRAGON INFORMATION PAPER

Surface hardness reinforced coating and preparation method thereof

The invention relates to a surface hardness reinforced coating and a preparation method thereof, and the reinforced coating is composed of a titanium carbide layer and a graphite layer. The preparation method comprises the following steps: (1) ultrasonic cleaning metal titanium or titanium alloy and drying in air by utilizing alcohol and acetone; (2) putting the metal titanium or titanium alloy into plasma reinforced chemical vapor deposition equipment, utilizing a mechanical pump to perform vacuum-pumping until vacuum degree is lower than 1*10<-1>Pa; (3) leading in argon gas of 200 sccm-400 sccm, and heating to 500-900 DEG C at a rate being 3 DEG C / min to 10 DEG C / min; (4) leading in methane gas of 10-50 sccm, closing argon gas, opening a radio frequency source, setting radio frequency power to be 100W-300W, and growing for 0.5-2 hours; and (5) closing the radio frequency source, leading in argon gas of 200 sccm-400 sccm, stopping to lead in methane gas, naturally cooling to the roomtemperature, thereby obtaining the titanium carbide / graphite reinforced coating. The proportion of titanium carbide to the graphite is regulated by controlling parameters such as methane gas flow andgrowth time, so that the performance of the coating is modulated.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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