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126results about How to "Short energy consumption" patented technology

Manufacturing method of negative plate of safety lithium-ion battery

InactiveCN106450169AGood thermal stabilityStable performance during charge and discharge cyclesSecondary cellsElectrode collector coatingCopper foilCurrent collector
The invention discloses a manufacturing method of a negative plate of a safety lithium-ion battery. The method comprises the steps of mixing a negative active material with a conductive agent at a certain mass ratio to obtain a mixture A; carrying out ball-milling and mixing on an additive B and the mixture A at a certain mass ratio to form a mixture C; preparing a certain mass percent of water solution from CMC which accounts for a certain mass ratio of the mixture C, carrying out constant-temperature stirring, adding an SBR which accounts for a certain mass ratio of the mixture C in batches, simultaneously adding an NMP which accounts for a certain ratio of the mixture C and carrying out constant-temperature stirring to form a sizing material D; adding the mixture C to the sizing material D in batches, controlling the solid content of the mixture C and stirring to obtain slurry; adding a proper amount of water, adjusting, controlling the viscosity and stirring to obtain negative slurry E; employing copper foil as a current collector F, intermittently coating a single side or double sides of the current collector F with the negative slurry E, reserving a certain current collector, carrying out drying, controlling the surface density, carrying out rolling and controlling the compactness and the thickness of the negative plate; and dividing, cutting, welding and pasting a tab adhesive tape to obtain the negative plate of the safety lithium-ion battery. The lithium-ion battery assembled by the negative plate has good electric cycle performance and safety performance.
Owner:HUBEI UEE ENERGY TECH CO LTD

Polymerization type phosphorus-containing flame retardant as well as preparation method and application thereof as epoxy resin flame retardant

The invention discloses a polymerization type phosphorus-containing flame retardant as well as a preparation method and application thereof as an epoxy resin flame retardant, relates to a hydrolysis-resisting phosphorus-containing flame retardant and a preparation method thereof, and solves the problems that a conventional phosphorus-containing flame retardant is low in thermal stability, easy to hydrolyte and hard to process. The structural formula of the phosphorus-containing flame retardant is as shown in the specification. The preparation method comprises the following steps: by taking phosphoric acid or sulfuric acid as a catalyst, adding a trisphosphine oxide solution or a tertphosphine oxide solution, a reaction solvent and an additive into a reaction container, adding a melamine or amine compound at the room temperature, adjusting the pH value, heating at a certain stirring speed, reacting at certain temperature, performing backflow reaction, cooling to be the room temperature, sequentially performing suction filtration, washing in water and drying, thereby obtaining white powder solid, that is, the polymerization type phosphorus-containing flame retardant. The polymerized type phosphorus-containing flame retardant can be used as the epoxy resin flame retardant which is added into epoxy resin.
Owner:NORTHEAST FORESTRY UNIVERSITY

High-magnetic-induction oriented silicon steel prepared through thin slab continuous casting and rolling and preparation method thereof

ActiveCN103774042ALow heating temperatureAvoiding Insufficient Inhibition ProblemsChemical compositionThin slab
The invention provides high-magnetic-induction oriented silicon steel prepared through thin slab continuous casting and rolling and a preparation method thereof. The oriented silicon steel comprises the following chemical components by mass percent: 0.035-0.055% of C, 2.9-3.3% of Si, 0.09-0.15% of Mn, 0.1-0.2% of Cu, not more than 0.005% of S, 0.02-0.04% of AlS, 0.009-0.013% of N and 0.1-0.2% of Sn. The oriented silicon steel is prepared by the following steps: thin slab continuous casting, heating in a soaking pit, hot continuous rolling, normalizing, primary cold rolling, decarburizing annealing and high temperature annealing, wherein the heating temperature of the soaking pit is 1150-1180 DEG C and the soaking time is 30-60 minutes. The oriented silicon steel uses AlN as a main inhibitor and Cu2S as an auxiliary inhibitor, and meanwhile, the trace element Sn is added to the chemical components to avoid the problem of inadequate inhibiting capacities of the inhibitors caused by low temperature heating and serves as an auxiliary inhibitor thanks to the segregation capacity of Sn on the grain boundary. Therefore, the high-magnetic-induction oriented silicon steel can be produced by adopting the thin slab low temperature short-time soaking process, so that the casting blank heating temperature is effectively reduced and the soaking time is reduced. The preparation method has the advantages of short flow, low cost, low energy consumption, high production efficiency and the like.
Owner:CENT IRON & STEEL RES INST +1

Method for preparing Chinese medicinal granules for treating cold

The invention discloses a method for preparing Chinese medicinal granules for treating a cold, which belongs to the field of medicine and overcomes the defects of low extraction rate of the conventional preparation method and high effective ingredient loss of medicaments. The preparation method comprises the following steps of: crushing schizonepeta spike, mint and perilla leaf into coarse powderaccording to a formula of cold heat clearing granules (No.1-644, version 2005), and extracting the medicaments with volatile oil by adopting supercritical CO2 and ultrahigh pressure; crushing bupleurum, parsnip, kudzuvine root, platycodon root, bitter almond kernel, angelica dahurica, bunge's corydalis and reed rhizome into coarse powder, mixing the coarse powder and the rest medicament residue of the extracted medicaments, performing ultrahigh pressure extraction by adding water, filtering the extract, and concentrating the extract with reduced pressure to form clear paste; and adding auxiliary materials into the clear paste to prepare granules, and adding volatile oil into the granules to obtain the Chinese medicinal granules. The method has the advantages of preventing oxidation, dissipation and reaction of thermo-sensitive components, completely keeping the bioactivity of biomass and reducing loss of effective ingredients along with quicker medicament response and stronger function.
Owner:XIUZHENG PHARMA GROUP HOIDING +1

Method for preparing tungsten molybdenum copper composite material by microwave sintering

InactiveCN109207762AReduce thermal stressThermal stress is minimizedThermal treatmentBall mill
The invention discloses a method for preparing a tungsten molybdenum copper composite material by microwave sintering. The method comprises the steps: firstly, ball milling tungsten powder, molybdenumpowder and copper powder, fully and evenly mixing, putting the evenly-mixed powder into a mold and pressing the evenly-mixed powder into a green body of a cylindrical structure; then putting the green body into a microwave sintering furnace and utilizing a specific thermal treatment technology to prepare the tungsten molybdenum copper composite material under a lower temperature. Directed to theproblems of a traditional method for preparing tungsten molybdenum copper alloy in the prior art, the invention provides the method for preparing the tungsten molybdenum copper composite material by microwave sintering. Compared with the existing traditional method, the method can reduce a preparation temperature to 700 to 1,000 DEG C from 1,100 to 1,600 DEG C and further can shorten the preparation time to 20 to 50 min from 100 to 760 min; furthermore, the method disclosed by the invention can finish a densification process only through three steps of powder mixing, pressing and sintering, sothat a technology is simplified, easiness in implementation is achieved, and a product with finer and evener grains and an excellent mechanical property can be obtained. The defects of high sinteringtemperature, long sintering time, complex technology and the like of the existing traditional sintering method are solved.
Owner:SICHUAN UNIV

Method for improving radial structure and performance uniformity of G115 steel large-caliber thick-wall pipe

ActiveCN108950148AImprove radial temperature fieldImprove uniformityFurnace typesHeat treatment furnacesQuenchingCaliber
The invention discloses a method for improving radial structure and performance uniformity of a G115 steel large-caliber thick-wall pipe, and belongs to the technical field of steel materials. The process comprises the following steps of a normalizing system and a tempering system, wherein the normalizing system is characterized in that a tube blank subjected to hot-extrusion is adopted, chargingis carried out by using the temperature of 400-600 DEG C, warming is carried out with the heating speed of 100-120 DEG C/h until the temperature reaches 980-1000 DEG C, the hardening time is 0.5-1 min/mm, then warming is carried out with the heating speed of 130-150 DEG C until the temperature reaches 1030-1080 DEG C, then hardening is carried out, the hardening time is 0.5-0.8 min/mm, heat preservation is carried out for 1-3 hours after hardening, and air cooling or water quenching is carried out to the room temperature; and the tempering system is characterized in that charging is carried out by using the temperature less than or equal to 600 DEG C, warming is carried out with the heating speed of 120-150 DEG C/h until the tempering temperature reaches 780 +/- 10 DEG C, the time of heatpreservation is 3-5 hours, and air cooling is carried out to the room temperature. The method has the advantages that the radial temperature field of the thick-wall pipe is improved, moreover, the grain of the thick-wall pipe is not prone to coarsening, so that the radial structure and performance uniformity of the thick-wall pipe is greatly improved.
Owner:CENT IRON & STEEL RES INST

Metal organic framework modified stannous sulfide composite photocatalyst as well as preparation method and application thereof

The invention discloses a metal organic framework modified stannous sulfide composite photocatalyst as well as a preparation method and application thereof. The composite photocatalyst takes a metal organic framework MIL-53(Fe) as a carrier and is loaded with stannous sulfide. The preparation method of the composite photocatalyst comprises the following steps: mixing MIL-53(Fe) with stannous sulfide, adding solution containing S<2->, and carrying out precipitation reaction, so that the metal organic framework modified stannous sulfide composite photocatalyst is obtained. The composite photocatalyst disclosed by the invention has the advantages of environment friendliness, large specific surface area, many reaction sites, high photogenerated electron-hole utilization rate, high photocatalytic activity, good stability and corrosion resistance, and the preparation method has the advantages of simplicity in operation, low raw material cost, low energy consumption, short consumed time and easy-to-control conditions. The composite photocatalyst disclosed by the invention can be used for degrading hexavalent chromium wastewater, has the advantages of high degradation efficiency, simple application method, low cost and no secondary pollution and has a good practical application prospect.
Owner:HUNAN UNIV

Preparation method of edible packaging film based on diatom polysaccharide

The invention discloses a preparation method of an edible packaging film based on diatom polysaccharide. The preparation method specifically comprises the following steps: degreasing diatom powder, concretely adding a chloroform methanol mixed solution into the diatom powder, carrying out degreasing, suction filtration, and drying to obtain degreased diatom powder; preparing the diatom polysaccharide, concretely uniformly mixing the degreased diatom powder with water, then adding 8-chlorotheophylline, and carrying out ultrahigh-pressure extraction and suction filtration, wherein the obtained filtrate is the water extracted crude polysaccharide; and preparing the edible packaging film, concretely taking the following components in parts by weight: the diatom polysaccharide, glycerol, gelatin, tea polyphenol and water, dissolving the components to prepare a film liquid, carrying out degassing, then uniformly pouring the degassed film liquid into a mold, and carrying out drying for forming a film, so as to obtain the edible packaging film. The preparation method disclosed by the invention has the beneficial effects that the preparation method is simple and feasible, the time consumption is low, the energy consumption is low, the utilization rate of the raw materials can be improved, and the degradable pollution-free packaging film with good performance can be formed. The surface of the packaging film is smooth and compact, the film is easy to uncover, and the packaging film is edible, is easy for industrial scale production and has good application value and market potential.
Owner:金华市铁骑士生物科技有限公司

Method for extracting ginsenoside by biomimetic method and ginsenoside extract by using method

The invention discloses a method for extracting ginsenoside by a biomimetic method and a ginsenoside extract by using the method. The extraction method comprises the steps of preparation of a biomimetic extraction solvent, biomimetic extraction of ginsenoside and extraction of an extracting liquid, wherein the biomimetic extraction solvent is biotic gastric juice or biotic intestinal juice; in thestep of biomimetic extraction of ginsenoside, ginseng is extracted by utilizing the prepared biomimetic extraction solvent after being dried and ground, the extracting liquid is centrifuged and filtered, and the extraction solvent is utilized to extract; in the step of extraction of the extracting liquid, the extracting liquid and the extraction solvent are mixed and separated, and the ginsenoside extract is obtained after the extracting liquid volatized and dried. by utilizing the biomimetic extraction method, the ginsenoside extract has high content of effective ingredients. Compared with atraditional organic solvent extraction method, the method has the characteristics of environmental friendliness, no toxicity or harm and high extraction efficiency. The method is low in energy consumption, short in time consumption, small in solvent consumption and simple and convenient to operate, has good accuracy, repeatability and precision, and is applicable to industrial production.
Owner:CHANGCHUN UNIV OF CHINESE MEDICINE

Micron-scale spheroidal ferric fluoride positive electrode material and preparation method thereof

The invention specifically relates to a micron-scale spheroidal ferric fluoride positive electrode material and a preparation method thereof. The micron-scale spheroidal ferric fluoride positive electrode material is prepared from a water / alcohol mixed solution of a ferric salt and a fluorine-containing aqueous solution. The preparation method is performed at a normal temperature and under a normal pressure, the preparation process is simple, the consuming time is short, the energy consumption is low, the cost is low, the environment-friendly effect is achieved, and the industrial production can be realized easily; the prepared FeF3(H2O)0.33 particles are spheroidal at the micron scale; the tap density of the material is improved; the material has excellent mobility, dispersibility and machinability, and is applicable to producing a positive electrode material slurry and coating an electrode plate; meanwhile, the material has a one-dimensional tunnel structure and is beneficial to the migration of lithium ions, so that the electrical conductivity of the material can be improved; in addition, the stability of the FeF3 structure is maintained in the charging / discharging process by use of little crystal water, and therefore, good electrochemical properties can be realized.
Owner:SHANDONG YUHUANG NEW ENERGY TECH +1

Bismuth molybdate/titanium carbide heterojunction two-dimensional photocatalytic material as well as preparation method and application thereof

The invention discloses a bismuth molybdate / titanium carbide heterojunction two-dimensional photocatalytic material as well as a preparation method and application thereof. The two-dimensional photocatalytic material includes titanium carbide nanosheets and layered bismuth molybdate supported on the titanium carbide nanosheets. The preparation method includes the following steps: preparing bulk titanium carbide; preparing the titanium carbide nanosheets by using dimethyl sulfoxide; and preparing the above two-dimensional photocatalytic material through a hydrothermal reaction. The two-dimensional photocatalytic material has the advantages of low costs, easy availability, low recombination efficiency of photoelectrons and holes, strong catalytic performance, good redox activity, and less harm to the environment, is a green and economic photocatalytic material, can be widely used to treat pollutants in the environment, and has higher use value and better application prospects; and the preparation method provided by the invention has the advantages of a simple process, convenient operation, low raw material costs, low energy consumption, short consumed time, mild easily controlled reaction conditions, greenness and environmental protection, and shows good application prospects in synthesis of functional nanomaterials.
Owner:HUNAN UNIV

Method for recycling rhodium from rhodium octanoate mother liquor

The invention relates to the technical field of precious metal recycling, and particularly discloses a method for recycling rhodium from rhodium octanoate mother liquor. The method includes the following steps that the rhodium octanoate mother liquor is subjected to slurry-mixing with acetic acid to obtain slurry; after the slurry, an oxidizing agent, and water are mixed, supercritical oxidation treatment is carried out, a gas-phase system and a non-gas-phase system are obtained through gas-liquid separation, the non-gas-phase system is subjected to solid-liquid separation treatment, and a first solid phase is obtained; the first solid phase is subjected to acid pickling treatment to obtain a second solid phase, a mixed system after acid pickling is collected to perform solid-liquid separation to obtain a third solid phase, and the second solid phase and the third solid phase are combined to obtain a rhodium crude product; and the rhodium crude product is washed to obtain the preciousmetal rhodium. The method is simple in technological process, low in pollution since organic matter is rapidly oxidized into innoxious substances such as carbon dioxide and nitrogen, short in processing time, low in energy consumption, and high in recovery rate, the loss of the precious metal rhodium is reduced, and the industrialization is easy.
Owner:南京新奥环保技术有限公司

Method for preparing enzyme by using honeysuckle and curcuma longa as main raw materials

The invention relates to a method for preparing an enzyme by using honeysuckle and curcuma longa as main raw materials. The method specifically comprises: (1) selecting 35-45 parts by weight of honeysuckle, 10-15 parts by weight of musa basjoo siebold, 10-15 parts by weight of pineapple, and 10-15 parts by weight of clausena lansium, and washing with clear water so as to be spare; (2) peeling the clausena lansium to expose the flesh, cutting the pineapple with the peel and the musa basjoo siebold with the peel into pineapple slices with the thickness of 1-2 cm and musa basjoo siebold slices with the thickness of 1-2 cm, and uniformly mixing the slices to obtain a mixture; (3) placing the mixture into a sealed container, adding honey and water, uniformly mixing, placing into a room, carrying out sealed fermentation at a room temperature, and maintain for 1 month, wherein stirring is performed everyday at the starting 5-7 days and stirring is performed every 7 days at the later days; and (4) washing fresh curcuma longa picked before and after winter solstice, cutting into curcuma longa slices with the thickness of 0.3-2 cm, taking 15-25 parts by weight of the curcuma longa slices, adding to the sealed container, and carrying out sealed fermentation for more than 3 months so as to obtain the product. According to the present invention, the enzyme prepared through the method has advantages of original food function maintaining, rich probiotics, rich nutrition, good taste, and long shelf life.
Owner:唐妙红
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