The invention relates to a preparation method of an attapulgite / fluorinated
polyurethane nanocomposite. The method comprises the steps of firstly, carrying out pretreatment on attapulgite, specifically, dispersing the attapulgite into deionized water, adding a dispersing agent-
sodium hexametaphosphate into the deionized water, stirring and then centrifuging,
drying and then
grinding, acidizing the purified attapulgite, and then carrying out centrifugal
drying and sieving; secondly, carrying out organic modification on the attapulgite, specifically, firstly hydrolyzing a
silane coupling agent KH550, then adding
alcohol and the pretreated attapulgite, carrying out a
reflux reaction and then filtering,
drying the obtained
filter cake,
grinding and sieving to obtain modified attapulgite; finally, evenly mixing fluorinated polyether
polyol and the modified attapulgite in a
nitrogen atmosphere condition, then adding
isocyanate into the mixture, heating, carrying out a reaction and then vacuumizing, removing bubbles, adding a chain
extender-
triethanolamine, stirring and then molding by vacuum solidification. The preparation method is mild in conditions, simple and convenient in operation, easy in control of conditions and low in cost.