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108results about How to "Achieve self-assembly" patented technology

Nucleic acid nano structure carrier-precious metal photosensitive contrast agent composite for living organism photo-acoustic imaging, preparation method and applications thereof

The invention discloses a nucleic acid nano structure carrier, a nucleic acid nano structure carrier-precious metal photosensitive contrast agent composite comprising the same, and preparation methods and applications of the carrier and the composite. The nucleic acid nano structure is a random two-dimensional and/or three-dimensional nano structure constructed by a DNA paper-folding technology. The precious metal components are used to carry out DNA modification on the surface of the carrier and selected from one or more of gold nano rods, gold nano shells, silver-coated gold nano rods, and gold nano cages. The provided composite is used as a photo-acoustic imaging probe, is capable of guaranteeing the absorption contrast enhancing effect of the photo-acoustic contrast agent which is coupled to the composite, and moreover can prominently improve the targeting performance of the contrast agent on tumors. Furthermore, the precious metal photosensitive components which are coupled to the carrier are enriched in the inner of tumor tissues, and thus the solved is the problems that conventional contrast agent is distributed over the whole human body or the contrast agent can only stay on the tumor surfaces. The preparation method has the advantages of simple technology, low cost, convenience, and easy application.
Owner:THE NAT CENT FOR NANOSCI & TECH NCNST OF CHINA +1

Resistive flexible strain sensor based on drying-mediated self-assembly, and preparation method of resistive flexible strain sensor

The invention relates to a resistive flexible strain sensor based on drying-mediated self-assembly of colloidal particles into parallel cracks, and a preparation method of the resistive flexible strain sensor. The flexible strain sensor comprises a flexible substrate, a sensitive layer and a conductive layer which are arranged from bottom to top in sequence, wherein the flexible substrate is a thin film made of a flexible material; the sensitive layer is prepared from a thin film produced through drying of colloidal dispersions, and the upper surface of the sensitive layer is provided with a regular crack array structure; a pair of copper sheet electrodes are arranged on the conductive layer, and are respectively located at the two ends of the conductive layer; and an enameled wire is ledout of each electrode. The flexible strain sensor provided by the invention can be adhered to the surface of human skin or attached to clothes to achieve wearable monitoring of respiration, pulses, gaits, joint movements and the like of a human body; and through the drying-mediated method, the colloidal particles are self-assembled into the parallel cracks, so that the flexible strain sensor has the characteristics of high sensitivity, high speed and high efficiency of a preparation process, high simplicity and environmental friendliness of a preparation technique, high convenience in mass production, low cost and the like, and achieves broad application prospects.
Owner:JILIN UNIV

Preparation method and application of shewanella spp-nanometer ferrous sulfide capsules

The invention belongs to the technical field of biology, and relates to a preparation method and application of shewanella spp-nanometer ferrous sulfide capsules. The method comprises the steps that an LB culturing medium and an M9 culturing medium are prepared, shewanella spp is inoculated to the LB culturing medium for culturing, and bacterial liquid is obtained; the LB culturing medium and theM9 culturing medium are mixed, sodium lactate, calcium chloride and magnesium sulfate are added, and reaction buffering liquid is obtained; then, the bacterial liquid is centrifuged, bacterial sludgeis added into the reaction buffering liquid until the OD 600 value is 0.05-5; then, a ferric chloride solution and a sodium thiosulfate solution are added into the reaction buffering liquid after inoculation of the bacterial sludge, and after culturing, centrifugation, washing and resuspending, the shewanella spp-nanometer ferrous sulfide capsules are obtained; in the process of synthesizing the capsules, the activity of the biological metabolism mechanism is fully utilized, the raw materials are simple and cheap, the application cost is low, and quantization production can be achieved; multi-period efficient removal for hexavalent chromium is efficiently achieved, and a new method is provided for efficiently processing heavy metal pollution.
Owner:JIANGSU UNIV

Stimuli-responsive type nucleic acid nanostructure carrier chiral noble metal nanocomposite and preparation method thereof and application

The invention discloses a nucleic acid nanostructure carrier, a stimuli-responsive type nucleic acid nanostructure carrier chiral noble metal nanocomposite comprising the same and a preparation method thereof and application. The nucleic acid nanostructure carrier is of two-triangular DNA paper folding structure constructed through a DNA paper folding technology, and the two triangular DNAs are connected through a control chain to form a rhombic paper folding structure. Concretely, the nucleic acid nanostructure carrier is of a nucleic acid nano-structure formed by self-assembly through hybridization of a scaffold chain and an auxiliary folding staple chain and hybridization of a control chain and the scaffold chain of the two-triangular DNA paper folding structure respectively. On the one hand, the stimuli-responsive type nucleic acid nanostructure carrier chiral noble metal nanocomposite overcomes shortcomings of optical signal modulation through a conventional plasma assembly (chain accumulation and limited adjustment range); on the other hand, a plasma structure is adjusted through an external environment, and the nucleic acid nanostructure carrier can be used for monitoring specific bioactive substances and the like.
Owner:THE NAT CENT FOR NANOSCI & TECH NCNST OF CHINA

Carbon-wrapped polyhedron silver nano-particle and controllable self-assembly preparation method thereof

ActiveCN104174865ASimple stepsImprove chemical reactivity and thermal stabilityNanotechnologyIonCarbon film
The invention discloses a carbon-wrapped polyhedron silver nano-particle and a controllable self-assembly preparation method thereof. A one-step water heating technology is adopted, glucose serves as a reducing agent and a carbon source, and polyvinylpyrrolidone (PVP) serves as a morphological control agent for metallic silver growth and triggers self-assembly of composite particles. The method for preparing the carbon-wrapped polyhedron silver nano-particle comprises the following steps: sequentially dissolving 1.0-2.0g of glucose, 0.25-2.80g of PVP and 0.02-0.04g of silver nitrate in 100ml of deionized water, and ultrasonically dissolving a solid for 20 minutes until the solid is completely dissolved; transferring 40ml of mixed solution into a 50ml reaction kettle, performing constant-temperature reaction for 6 hours at a certain temperature of 160-200 DEG C, and cleaning and drying a product. According to the self-assembly of the composite nano-particles, other conditions are unchanged, the concentration of the PVP is increased to reach a certain value, and the suspension liquid of the cleaned product is directly added to the surface of a carbon film, a silicon chip or other carriers dropwise. The method has a simple process, is low in cost and easy to industrialize, and can be popularized to preparation and industrialized production of other core-shell structure nano-particles and self-assembly structures.
Owner:NANJING UNIV

Polyethylene glycol grafted graphene oxide composite solid-solid phase change material and preparation method thereof

InactiveCN108410426AAchieve self-assemblyRealization of graft polymerized polyethylene glycolHeat-exchange elementsSolid phasesLayered structure
The invention discloses a polyethylene glycol grafted graphene oxide composite solid-solid phase change material. The main components comprise polyethylene glycol, a crosslinking agent and graphene oxide; the polyethylene glycol is subjected to tail end functionalized modification by the crosslinking agent; the polyethylene glycol and the graphene oxide form a mutually linked skeleton through electrostatic interaction between a hydrogen bond and a functional group; and the polyethylene glycol grafted graphene oxide composite solid-solid phase change material has a graphene layered structure. The preparation method comprises the following steps: 1) performing molecular chain tail end functionalized modification on the polyethylene glycol by the crosslinking agent; and 2) adding the grapheneoxide to perform self assembling and graft polymerization on the polyethylene glycol. Self assembling of the graphene oxide and graft polymerization of the polyethylene glycol are realized through molecular chain tail end functionalization, a composite phase change material with a graphene layered structure is formed, and the advantages of maintaining solid state in the phase change process, obviously improving phase change latent heat and having more excellent heat conductivity are achieved. Therefore, the polyethylene glycol grafted graphene oxide composite solid-solid phase change materialhas a wide application prospect in the field of phase change thermal storage.
Owner:GUILIN UNIV OF ELECTRONIC TECH

Butterfly-shaped SnO2 two-dimensional nanometer material, and preparation method and application thereof

The invention discloses a butterfly-shaped SnO2 two-dimensional nanometer material, and a preparation method and an application thereof. The butterfly-shaped SnO2 two-dimensional nanometer material isprepared by using SnSO4 and SDBS as raw materials through a two-step combined method of a hydrothermal reaction and high-temperature oxidizing annealing. The butterfly-shaped SnO2 two-dimensional nanometer material has a two-dimensional butterfly shape and a structure rich in surface defects, and has the characteristics of gas adsorption, surface activity, oxidation reduction and gas sensitivity.The preparation method comprises the following steps: preparation of a precursor solution, a main reaction, separation of a precursor, and preparation of a nanometer material through high-temperatureoxidizing heat treatment. The application comprises the application of the butterfly-shaped SnO2 two-dimensional nanometer material in preparation of gas sensors. Directed at the problems of complicated preparation procedures, high cost, incapability of realizing large-scale preparation and addition of environmentally-unfriendly, toxic and harmful organic solvents like strong acid and strong alkali in conventional preparation of the two-dimensional SnO2 nanometer material, the invention provides a simple, economical, green and easily-scaled synthetic method.
Owner:YUNNAN UNIV

Sugar-containing amphiphilic segmented copolymer and preparation method thereof

The invention discloses a sugar-containing amphiphilic segmented copolymer and also discloses a preparation method of the sugar-containing amphiphilic segmented copolymer. The preparation method specifically comprises the following steps: firstly, a macromolecular chain transfer agent is prepared by a ring opening polymerization method; then, by a reversible addition-fragmentation chain transfer polymerization method and under the action of the macromolecular chain transfer agent, active monomer unsaturated pentafluorophenyl ester polymerization is initiated to prepare an amphiphilic segmented copolymer; and finally, by an active pentafluorophenyl ester-amino reaction method, the segmented copolymer and a sugar-containing polymer containing an amino group react to generate the sugar-containing amphiphilic segmented copolymer. According to the method, the defect that traditional sugar-containing polymer synthesis has complicated steps for preparation of an unsaturated sugar-containing monomer is overcome; reaction steps of the method are simplified; reaction conditions are mild; and the type of a sugar-containing polymer containing an amino group can be selected. The sugar-containing amphiphilic segmented copolymer of the invention has potential application in the aspects of controlled release of drugs and targeting therapy of tumor.
Owner:SOUTHWEST UNIV

Method for preparing transition metal oxide positive electrode material of lithium

The invention relates to a method for preparing a transition metal oxide positive electrode material of lithium. The method is a metal-organic coordination polymer precursor method, and the transition metal oxide of lithium can be prepared by performing thermal treatment and high-temperature calcination to the metal-organic coordination polymer. The transition metal oxide of the lithium prepared by using the method is good in crystal form, has nanoscale, special morphology and specific crystal orientation, and can show excellent electrochemical performance when being used as a positive electrode material of a lithium ion battery. The LiNi0.5Mn1.5O4 synthesized by using a method and having a spinel structure can achieve the specific capacity up to 117mAh/g when being used for discharging at 10 DEG C and 40 DEG C, and the specific capacity can be kept above 81.0% after being cyclized for 500 times. The specific capacity can achieve 105mAh/g after charging and discharging are carried out for 350 times according to 1C rate at 55 DEG C. In addition, the lithium-rich manganese-based positive electrode material 0.3Li2MnO3.0.7LiNi0.5Mn0.5O2 prepared by utilizing the method and having a laminar structure has reversible specific capacity. Two classes of materials are used as the positive electrode materials of the lithium ion battery with high specific energy and high specific power, and the method has wide application prospects.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Molecularly imprinted membrane for chiral separation and preparation method thereof

The invention discloses a molecularly imprinted membrane with a selective-separation chiral drug and a preparation method of the membrane. According to the invention, D-naproxen is taken as template molecules, a PVDF (Polyvinylidene Fluoride) hollow fiber separation membrane is taken as a base material, and the D-naproxen imprinted molecules are packaged in a fenestra grafting gel layer in a surface finish process to prepare the D-naproxen imprinted PVDF hollow fiber membrane. The molecularly imprinted separation membrane prepared by the method has good adsorption and separation functions to naproxen chiral drug molecules, has a desorption rate up to 90%-95.78%, can realize the intelligent regulation and control on combination and release of D-naproxen and solves the problem of uncontrollability on the shape and size of cavities and the affinity of template molecules of the conventional molecularly imprinted membrane. According to the invention, the mature PVDF hollow fiber membrane on the market is taken as a base membrane of the molecularly imprinted membrane, and an N-isopropyl acrylamide monomer (NIPAAm) of the conventional thermo-sensitive hydrogel is taken as a functional monomer; and the preparation method is simple, low in production cost as not needing special equipment, and suitable for industrialized application.
Owner:TIANJIN POLYTECHNIC UNIV

Porous carbon fiber loading transition metal oxide, biosensor and preparing method of porous carbon fiber loading transition metal oxide

The invention discloses a porous carbon fiber loading transition metal oxide, a biosensor and a preparing method of the porous carbon fiber loading transition metal oxide and belongs to the technicalfield of biosensors. The porous carbon fiber loading the transition metal oxide is prepared in the manner that high-molecular polymers, transition metal salt and a solvent are mixed to obtain a spinning precursor solution, and then carbonization treatment is conducted after electrostatic spinning. The biosensor is prepared in the manner that boric acid base electric conducting polymers are fixed with the porous carbon fiber as the base body. The porous carbon fiber loading the transition metal oxide is provided with a uniform mesoporous structure, holes communicate with one another, subsequenttreatment is not needed, the preparing technology is simple, and repeatability is high. The boric acid base electric conducting polymers are fixedly loaded on the surface of the porous carbon fiber loading the transition metal oxide and can serve as the transmission medium of electric charges, meanwhile, the electric conduction performance and the biological recognition performance of the boric acid base electric conducting polymers can promote the charge transmission capability and the specificity selectivity of an electro-catalysis reaction, and response signals of the electro-catalysis reaction are improved.
Owner:SHANDONG ANRAN NANOMETRE IND DEV CO LTD +1

Sulfur/polypyrrole/graphene/carbon nanotube composite film and preparation method and application thereof

ActiveCN110459755AFacilitate partial reductionPromotes oligomerizationSecondary cellsPositive electrodesComposite filmFiltration
The invention provides a sulfur / polypyrrole / graphene / carbon nanotube composite film and a preparation method and an application thereof, and belongs to the technical field of chemical energy storage batteries. Polypyrrole in the film is grafted on reduced graphene oxide; the reduced graphene oxide and the functionalized carbon nanotubes are interwoven to form a three-dimensional carbon framework;and elemental sulfur is loaded in the three-dimensional carbon framework. According to the method, self-assembly is initiated by using an oxidation-reduction reaction between pyrrole and graphene oxide. Meanwhile, the functionalized multi-walled carbon nanotubes serve as a second carbon framework to provide an ion / electron rapid transmission channel, and a flexible self-supporting composite film is constructed through one-step vacuum filtration and post-sulfur loading. By using the strong adsorption of polypyrrole to polysulfide and the synergistic effect of the interwoven three-dimensional conductive framework constructed by graphene and carbon nanotubes, the problems of inherent non-conductivity of elemental sulfur, shuttle effect of polysulfide and the like can be solved, and the electrochemical performance of the lithium-sulfur battery is further improved.
Owner:BEIJING INSTITUTE OF TECHNOLOGYGY

Method of constructing graphical magnetic micro-nano structure through laser beam direct writing

The invention provides a method of constructing graphical magnetic micro-nano structures through laser beam direct writing, wherein the method includes the following processes: (1) at least spreading more than one layers of magnetic material particles on a surface of a substrate, and then applying a controllable magnetic field so that the magnetic material particles are arranged orderly according to magnetic lines on the magnetic field on the surface of the substrate; (2) by means of the laser beam entering from one side of the back side of the substrate to scan the substrate, wherein the position irradiated by the laser beam absorbs laser energy so that the position is subjected to rapid temperature increasing, so that the irradiated position on the back side of the substrate is free of being molten or subjected to thin-layer melted while the parts on the magnetic material particles on the front side of the substrate is partially melted, and finally cooling the substrate to achieve welding between the magnetic material particles to the substrate; and (3) repeatedly doing the step (1) and the step (2) to prepare the micro-nano structure being multilayered, being different in size and being order. The method is used for preparing the graphical magnetic micro-nano structure, wherein the size and the shape of the micro-nano structure are controlled, so that super-hydrophobic property, electromagnetic wave absorption and reflection characters of the surface can be adjusted and controlled.
Owner:WENZHOU UNIVERSITY

Preparation of antibacterial structural color fibers based on silk protein and antibacterial structural color fabric

The invention relates to a preparation method of antibacterial structural color fibers based on silk protein. The preparation method comprises the following steps: dispersing colloidal microspheres inwater to prepare colloidal emulsion with mass fraction of 6 to 15 percent, wherein the colloidal microspheres are polystyrene microspheres, polymethylmethacrylate microspheres and titanium dioxide microspheres; dissolving the silk protein, cellulose and rare earth elements in an aqueous solution of alkali, and carrying out electrostatic spinning to obtain silk protein fibers; enabling the silk protein fibers to pass through the colloidal emulsion in a lifting way from bottom to top; drying moisture by airing. The invention also provides an antibacterial structural color fabric based on the silk protein. The antibacterial structural color fabric comprises a base fabric layer and an antibacterial coloring layer, wherein the base fabric layer is formed by weaving warp yarns and weft yarns; all weft yarns are connected between every two adjacent warp yarns in an inclined manner; at least one of each warp yarn and each weft yarn is used as a wrapping yarn; the wrapping yarns are prepared from silks and bast fibers; the bast fibers are core yarns; the silks cover the surfaces of the bast fibers; the antibacterial coloring layer is prepared from the antibacterial structural color fibersbased on the silk protein.
Owner:SUZHOU BEST COLOR ENVIRONMENTAL PROTECTION NANOTECH CO LTD
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