212 results about "Dimethylbenzenes" patented technology

The application relates to the technical field of concrete member protection, and particularly discloses a highway concrete member protection coating under a coastal environment and a preparation method thereof. The highway concrete member protection coating under the coastal environment comprises an epoxy resin bottom layer and a fluorocarbon resin surface layer, the fluorocarbon resin surface layer is formed by spraying a surface layer coating, and the surface layer coating comprises the following raw materials in parts by weight: 28-32 parts of fluorocarbon resin, 3-5 parts of graphene oxide, 6-10 parts of montmorillonite, 10-14 parts of a stabilizing component, 160-170 parts of dimethylbenzene, the stabilizing component comprises a toughening agent, a leveling agent and a compatilizer, and the weight ratio of the toughening agent, the leveling agent and the compatilizer is 2-3:2-3:1. The protection coating can be used for protecting highway concrete members under a coastal environment.

The present invention relates to the field of pharmaceutical chemistry, and discloses a salt of carebastine and its use, which solves the problems of the prior art, such as poor solid form of carebastine, many impurities, instability, difficulty in purification, difficulty in mass synthesis, and inapplicability to medicinal use. The salt of carebastine of the present invention includes, but is not limited to, acid salts or base salts, particularly potassium salt, sodium salt, methanesulfonate salt and p-toluenesulfonate salt. The salt of carebastine of the present invention is used in the preparation of drugs for histamine H1 receptor antagonists. The salt of carebastine of the present invention has the characteristics of easy purification, high stability, simple process, easy industrial production, and good hygroscopicity and convenient storage. And the salt of the present invention can enter the body quickly and exert its medicinal effect, has good oral absorption, and is superior to ebastine in both safety and individual variation, and is a promising anti-allergic disease drug for development.

The invention relates to the technical field of antistatic agents, and particularly discloses an oil product antistatic agent and a preparation method thereof. The modified polysulfone is obtained by mixing and treating the following raw materials in parts by mass: 35-40 parts of xylene, 20-25 parts of composite polyamine, 15-20 parts of polysulfone, 5-8 parts of oligomeric dopamine and 1-2 parts of an activating agent, the preparation method comprises the following steps: taking composite polyamine, mixing with oligomeric dopamine, dispersing with xylene, then adding an activator, stirring, then adding polysulfone, and continuously treating, thereby obtaining the product. The preparation method of the composite polyamine comprises the following steps: taking epichlorohydrin, dispersing, adding a mixed amine source, heating, adding sodium carbonate, continuously stirring, cooling, adding a deprotection agent, filtering after treatment, taking a liquid part, drying by distillation, washing, drying again, and grinding to obtain the composite polyamine. The oil product antistatic agent prepared by the invention has relatively strong antistatic capability and relatively long duration time, and can form a firmer double-electric-layer structure.

The invention provides a charcoal-loaded iron-based catalyst suitable for heterogeneous catalysis as well as a preparation method and application of the charcoal-loaded iron-based catalyst. The preparation method comprises the following steps: firstly, activating and modifying tea leaves by adopting a potassium hydroxide solution, and then carrying out heat-preservation pyrolysis in a carbon dioxide atmosphere to obtain tea-leaf-based biochar; uniformly mixing an iron source, a manganese source, a cerium source and a citric acid solution; adding tea-based biochar, uniformly mixing, and drying to obtain a precursor; and heating the precursor to 400-650 DEG C, and carrying out heat preservation and pyrolysis to obtain the biochar-loaded iron-based catalyst. The biochar-loaded iron-based catalyst has excellent degradation and removal effects and cycle stability on xylene.

The invention provides a bacteriostatic and scale-inhibiting PE material and a preparation method thereof, and belongs to the technical field of high polymer materials, the preparation method comprises the following preparation steps: dissolving polyethylene in xylene, dissolving, adding perfluorohexylethylene and dicumyl peroxide, reacting, precipitating, washing, and drying to obtain perfluoro modified PE; the preparation method comprises the following steps: dissolving four-arm polyethylene glycol amine in a PBS buffer solution, adding 4-carboxyphenylboronic acid, EDC.HCl and NHS, carrying out a stirring reaction in a dark place, carrying out ultrafiltration and freeze drying to obtain PBA-PEG, dissolving the PBA-PEG in a Tris-HCl buffer solution, adding dopamine hydrochloride, and carrying out mixing, oxidation reaction, dialysis purification and drying to obtain a PBA-DA-PEG compound; the preparation method comprises the following steps: pre-mixing perfluorinated modified PE, mixing with an antioxidant and a compatibilizer, injecting the PBA-DA-PEG compound, continuously mixing, extruding, and carrying out water-cooling pelletizing to obtain the antibacterial and scale-inhibiting PE material. According to the PE material obtained by the invention, the antibacterial performance and the scale inhibition performance of the material can be improved at the same time.

The invention relates to a preparation method of silicon dioxide-boron nitride nanobelt aerogel, which comprises the following steps: dissolving melamine and boric acid in a co-solvent of tert-butyl alcohol and hot deionized water, stirring and mixing, carrying out ultrasonic treatment, freeze-drying and the like to obtain a melamine-boric acid aerogel precursor, placing the precursor in a tubular furnace, and carrying out vacuum drying to obtain the silicon dioxide-boron nitride nanobelt aerogel. Pyrolyzing in an ammonia gas atmosphere to obtain boron nitride nanobelt aerogel; and placing the boron nitride nanobelt aerogel in a xylene solution containing tetraethoxysilane and silicon tetrachloride, taking out the boron nitride nanobelt aerogel, and drying the boron nitride nanobelt aerogel. And hydrolyzing and pyrolyzing in an inert atmosphere to form a silicon dioxide layer on the surface, thereby obtaining the silicon dioxide-boron nitride nanobelt aerogel. The silicon dioxide and boron nitride nanobelt aerogel is low in density and excellent in mechanical property and oxidation resistance.

The present application relates to a kind of powder coating hydroxyalkylamide matting curing agent and its preparation method, the matting curing agent using including citric acid, 2-methyl-1,3-propanediol, dimethylbenzene, anhydrous methanol, N-methyl monoethanolamine, catalyst, nanometer titanium dioxide is reacted to obtain raw materials.In first, citric acid and 2-methyl-1,3-propanediol are grafted to carry out reaction, then the remaining four carboxyl groups of grafting are methyl esterification reaction, obtain methyl esterification product, then with N-methyl monoethanolamine acylation reaction obtains hydroxyalkylamide curing agent;Add nanometer titanium dioxide, fully mix and process to obtain the matting curing agent.The curing agent product functionality is higher, the hardness of coating film after curing is higher, and the boiling water resistance is excellent;And the coating film after curing has obvious matting effect, coating film gloss is basically reached 50-70%, and the decorative property is excellent.

An subject of the present invention is (S)-2-Methyl-5-(1-methyl-2-pyrrolidinyl)pyridine for use in in a method for the treatment of nicotine dependence in an amount of 0.1-5% by weight, a pharmaceutical composition comprising (S)-2-Methyl-5-(1-methyl-2-pyrrolidinyl)pyridine for use in a method for the treatment of nicotine addiction in an amount of 0.1-5% by weight per composition of oral, inhalation and dermal products for humans. It is also an subject of the present invention to use a composition comprising (S)-2-Methyl-5-(1-methyl-2-pyrrolidinyl)pyridine in an amount of 0.1-5% by weight as a substitute for a nicotine composition in food products, inhalation and dermal products for humans, the composition being in liquid or solid form and selected from such as e-cigarettes, e-cigarette liquids, chewing tobaccos, oral pouches, chewing gums, candies, lollipops, strips, dragees, jelly beans, lozenges, tablets, snuffs, shisha-type smoking mixtures, toothpastes, inhalation mixtures, inhalers or skin patches.

The invention discloses high-wear-resistance HFBMA (hexafluorobutyl methacrylate) acrylic resin and a preparation method thereof. The high-wear-resistance HFBMA acrylic resin is prepared from the following components in percentage by mass: 30 to 40 percent of styrene, 8 to 15 percent of hydroxypropyl ester, 8 to 15 percent of propyl butyl ester, 0.3 to 1.5 percent of methacrylic acid, 0.5 to 2 percent of initiator, 3 to 10 percent of hexafluorobutyl methacrylate (HFBMA), 2 to 8 percent of organic silicon monomer or POSS (polyhedral oligomeric silsesquioxane) and 25 to 35 percent of xylene. According to the experiment, the optimal raw material composition and proportion are obtained through screening of a large number of experiments, the optimal synthesis process is obtained through optimization of a large number of experiments, and the conversion rate reaches 98.8% or above. The acrylic resin disclosed by the invention has excellent wear resistance, weather resistance, chemical resistance, high hardness, high adhesive force and excellent hydrophobicity and anti-fouling performance, and the comprehensive performance is remarkably and technically improved.

The invention relates to the technical field of catalysis, and discloses a combined catalyst and application thereof in preparation of 1, 4-cyclohexanedimethanol. The catalyst A and the cocatalyst in the combined catalyst have high reaction selectivity in the process of catalytically oxidizing paraxylene (PX) to prepare terephthalyl alcohol, so that the conversion rate of the PX and the yield of the terephthalyl alcohol are relatively high, and an oxidation product can be directly hydrogenated to prepare 1, 4-cyclohexanedimethanol without separation and purification; meanwhile, the hydrogenation catalytic performance of the catalyst B is excellent; under the combination, paraxylene can be directly converted into 1, 4-cyclohexanedimethanol through a one-step oxidation reaction and a one-step hydrogenation reaction, the technological process can be greatly shortened, and the catalyst is easy to separate and recover after reaction.

The invention provides a diesel oil anti-wear agent and a preparation process thereof, and belongs to the technical field of diesel oil additives, and the preparation process comprises the following steps: mixing and stirring diisooctyl maleate and xylene, adding diethylenetriamine and deionized water, carrying out heating reaction, adding toluene, 4-(aminomethyl) pyridine and ethylene oxide, carrying out mixing reaction, filtering, washing, and drying to obtain the diesel oil anti-wear agent. The pyridinium-based polyester hollow capsule is prepared; the preparation method comprises the following steps: mixing xylene, catechol, ethylene phosphonic acid, ammonium persulfate and deionized water, heating, dispersing in cyclohexane, adding polyvinyl alcohol, octadecyl methacrylate and azodiisobutyronitrile, mixing and reacting to obtain catechol phosphonate nano colloidal particles; mixing and stirring the fatty acid ester solution, the oleoyl fluorocarbon copolymer and the pyridinium-based polyester hollow capsule, adding the catechol phosphonate nano colloidal particles, continuously stirring, performing ultrasonic treatment, and degassing to obtain the diesel oil anti-wear agent. The diesel oil antiwear agent can improve the antiwear property and demulsibility of the diesel oil antiwear agent.

The invention provides a protective coating for a fuel storage and transportation cabin and a preparation method thereof, the protective coating comprises a primer layer, and the primer layer comprises a component A and a component B, the component A is prepared from the following raw materials in parts by weight: 20 to 40 parts of phosphorylated-sulfur heterocyclic modified epoxy resin, 0.1 to 1 part of dispersing agent, 0.1 to 1 part of flatting agent, 0.1 to 1 part of defoaming agent, 0 to 10 parts of n-butyl alcohol, 0 to 10 parts of xylene, 10 to 15 parts of zinc phosphate, 0.5 to 1.0 part of thixotropic agent, 10 to 15 parts of flaky filler, 20 to 35 parts of talcum powder, 5 to 10 parts of barite powder and 3 to 10 parts of titanium dioxide; the component B is prepared from the following raw materials in parts by weight: 99 to 100 parts of amino resin and 0.3 to 0.8 part of a catalyst. Phosphorylation-sulfur heterocycle is utilized to modify epoxy resin, a phosphating group (P-O-C) is generated, the lipophobicity is increased, an intrinsic anti-swelling network is constructed based on a sulfur / phosphorus atom covalent bonding epoxy skeleton, and by utilizing the three-dimensional shielding effect of phosphorus atoms and the high-density cross-linking characteristic of thioether bonds, the anti-swelling performance of the epoxy resin is improved. Fuel oil permeation channels are blocked from the molecular level, pollutant dissolution is inhibited, and it is ensured that the coating has good soaking resistance to fuel oil.

The invention discloses a low-damping PVC-U electrical conduit and a processing technology thereof, and belongs to the technical field of conduit preparation. The low-damping PVC-U electrical conduit is prepared from the following components in parts by weight: 70 to 80 parts of PVC resin, 30 to 42 parts of light calcium carbonate, 8 to 15 parts of ethylene-vinyl acetate copolymer, 0.5 to 1 part of ethylene bis stearamide, 3 to 6 parts of epoxy compound and 4 to 7 parts of compound stabilizer, the preparation method comprises the following steps: preparing an epoxy compound from ethyl benzoylacetate, 2-(trimethylsilyl) phenyl trifluoromethane sulfonate, p-toluenesulfonyl azide, p-aminophenol, p-toluenesulfonyl chloride, iodobenzene diacetic acid and rhodium diacetate as raw materials, and preparing the compound stabilizer from 2-(2-aminoethoxy) ethanol, 4-fluorophenol and xylene alkane diisocyanate as raw materials. The PVC-U electrical conduit prepared from the substances has the advantages of low damping, excellent stability, excellent mechanical property and excellent aging resistance.

The invention discloses a heat-conducting and insulating BN / Al2O3 / EVA photovoltaic packaging adhesive film, a preparation method and application, flaky boron nitride and spherical aluminum oxide are adopted as heat-conducting fillers, an ethylene vinyl acetate copolymer and the heat-conducting fillers are dispersed in xylene by adopting a high-speed shearing method, and glass is coated with the xylene in a blade coating manner, so that the heat-conducting and insulating photovoltaic packaging adhesive film is formed. The flaky boron nitride and the spherical aluminum oxide are in contact with each other to form a three-dimensional heat conduction path, and meanwhile, the shear strength of the packaging adhesive film is effectively improved due to the addition of the inorganic particles. The in-plane heat conductivity can reach 2.71 W / m.K, the out-plane heat conductivity can reach 1.01 W / m.K, heat conduction can be conducted quickly, and heat accumulation of the photovoltaic module is effectively relieved. Under the irradiation of sunlight, the photovoltaic module can be cooled by 2 DEG C, and the working voltage of 5 mV is increased. In addition, the packaging adhesive film has excellent electrical insulation property and mechanical property, and ensures stable and safe operation of the photovoltaic module in practical application.

The invention discloses weather-resistant and medium-resistant alkyd resin varnish and a preparation method thereof. The varnish is prepared from the following raw materials: modified alkyd resin, a composite drier, zirconium iso-octoate with the purity of 12%, an anti-skinning agent, 200 # solvent oil and xylene. The modified alkyd resin is prepared from the following raw materials: soya oil acid, pentaerythritol, benzoic acid, pyrrolidine-2-one-1-acetic acid, dimethylbenzene and a 200 # solvent. According to the invention, pyrrolidine-2-ketone-1-acetic acid is used as a binary acid component to partially or completely replace traditional phthalic anhydride, so that the reaction efficiency of alkyd resin synthesis can be improved, and the problems of yellowing, pulverization and poor water resistance of traditional alkyd resin can be solved; according to the varnish prepared by the invention, on the basis of maintaining the inherent gloss, flexibility and constructability of alkyd resin, the key properties such as weather resistance, water resistance and acid resistance are improved; the whole preparation process of the varnish continues to use mature alkyd resin production equipment and flow, and has good economical efficiency and industrial popularization prospects.

The invention discloses a kind of CO2 responsive type gemini imidazoline surfactant and its application in fracturing fluid, tetraethylene pentamine and long-chain fatty acid are fed, using the dimethylbenzene of mass equal to long-chain fatty acid as water-carrying agent, being warming up to 125~140 DEG C and being refluxed, then continuing to be warming up to 190~220 DEG C and being reversed, being cooled to room temperature successively, obtain gemini imidazoline viscous liquid;Step 2:3 chloro-2 hydroxypropyltrimethylammonium chloride and the composition solution of acetone of equal mass are added dropwise to the gemini imidazoline of step one while stirring, then equimolar acid binding agent is added, reacted at room temperature, being warming up to 56~60 DEG C and distilling out acetone, CO2 responsive type gemini imidazoline surfactant can be obtained.The present invention can be used for the thickening agent of clean fracturing fluid, while improving the viscoelasticity of surfactant as thickening agent for preparing clean fracturing fluid, and the clean fracturing fluid formed is obviously stronger acidic, can dissolve the inorganic blockages such as carbonate rock in partial stratum.

The application discloses a bifunctional catalyst for preparing p-xylene from carbon dioxide and hydrogen in one step, a preparation method and application, relates to the technical field of catalysts for preparing p-xylene from carbon dioxide and hydrogen, and opens up a new way for selectively hydrogenating carbon dioxide into high-value p-xylene; the application comprises alkali metal modified FeMn oxides and ZSM-5 capsule zeolites, and is used for converting CO2 into p-xylene through one-step hydrogenation; in the alkali metal modified FeMn oxides, Mn is dispersed on the oxide phase of Fe; the ZSM-5 capsule zeolites are subjected to hydrothermal treatment with a TPAOH solution, and the external passivated Bronsted acid sites of the ZSM-5 capsule zeolites can inhibit the structuralization reaction of dimethylbenzene; the bifunctional catalyst can realize the conversion of carbon dioxide into p-xylene in one step, has high carbon dioxide conversion rate, high space-time yield of p-xylene, and long catalyst service life.

The invention belongs to the technical field of coating protection, and particularly relates to a preparation method of a single-component high-temperature fast curing silver-aluminum polymer coating applied to the surface of a coating layer. Comprising 175-180 parts of modified epoxy resin; 95 to 100 parts of flaky aluminum silver powder; 180-200 parts of a mixed solvent of dimethylbenzene and / n-butyl alcohol; 100 to 120 parts of dicyandiamide; 25 to 40 parts of 3-(3, 4-dichlorophenyl)-1, 1-dimethylurea; 10 to 12 parts of sodium molybdate; 4-8 parts of graphite; 1 to 2 parts of polydimethylsiloxane; 2 to 6 parts of a wetting agent HY-352; 3-5 parts of fumed silica; 0.5 to 3 parts of dimethyl silicone oil; and 0.2-2 parts of a hydroxymethyl cellulose agent. The coating disclosed by the invention has the advantages of thin coating, high-temperature rapid curing, relatively good corrosion resistance, good combination with a coating layer and the like, and also has excellent storage stability.

A novel pesticide formulation comprising an adjuvant selected from diketopiperazines and a pesticide active substance. A concentrate suitable for forming the formulation is also provided. The diketopiperazine provides the adjuvant activity in the concentrate and the pesticide formulation. A method for making the formulation is also provided, as well as the use of the diketopiperazine as an adjuvant in a pesticide formulation. A method for forming the diketopiperazine is also described. The diketopiperazine can be used in formulations or seed coatings for treating plants to control pests.

A method and system or kit is provided, where makeup containing an alkane and a styrenic block copolymer can be easily removed if a separate makeup-removing composition that includes an alkane and a low viscosity dimethicone (having a viscosity of 60,000 cst or less) is applied. The dimethicone in this viscosity range causes the styrenic block copolymer to gel. After allowing a short period of time for the gelling to occur, the gelled copolymer and the remainder of the makeup can then be readily removed.

The present application relates to the technical field of fine chemicals synthesis, and discloses a method for high-selectivity co-production of phthaloyl chloride and benzoyl chloride. The method uses dimethylbenzene and trichlorobenzene as raw materials, and feeds them into a photochlorination reaction tower to heat the materials. Then, the reaction tower is kept in a micro-negative pressure condition to perform photochlorination reaction. After the reaction is completed, the liquid is directly fed into a reaction kettle, and phthalic acid and a catalyst are added. Finally, the reaction liquid is separated by rectification to obtain the products phthaloyl chloride and benzoyl chloride. The present application greatly improves the selectivity of dimethylbenzene photochlorination reaction, and inhibits the ring chlorination side reaction. The present application can realize flexible co-production of m-phthaloyl chloride and p-phthaloyl chloride and benzoyl chloride, and can flexibly adjust the generation ratio of phthaloyl chloride and benzoyl chloride according to the raw material supply and product demand, thereby greatly improving the production flexibility of the reaction device.

The application discloses high-crack-following epoxy paint for concrete, a coating layer, a preparation method and application thereof. The high-crack-following epoxy paint comprises an A component composed of G-clay modified epoxy resin, polydopamine, a polymer elastomer, a wetting dispersant, a grafting coupling agent, an anti-settling agent, a pigment and filler, butanol and dimethylbenzene, and a B component composed of a flexible curing agent, butanol and dimethylbenzene. The A component and the B component are uniformly mixed to obtain the high-crack-following epoxy paint for concrete. The application further discloses a high-crack-following epoxy coating layer formed by curing the high-crack-following epoxy paint for concrete. The high-crack-following epoxy paint for concrete and the high-crack-following epoxy coating layer have excellent high-crack-following property and have application prospects in the field of concrete structure engineering in C5 harsh environment.

The invention relates to the technical field of coatings, and discloses a heat insulation coating for a heat exchanger and a preparation process thereof.The preparation process comprises the following steps that epoxy resin and modified cardanol are added into xylene, stirring is conducted for 10-15 min at the speed of 600-800 r / min, stirring is kept, a dispersing agent, a defoaming agent, modified graphene and titanium dioxide are sequentially added into the xylene, high-speed dispersion is conducted for 20-30 min, then the rotating speed is reduced to 300-500 r / min, stirring is conducted for 20-30 min, and the heat insulation coating for the heat exchanger is obtained. Adding hollow glass beads into the mixture, stirring at a low speed for 8-10 minutes, finally adding a curing agent, continuously stirring for 5-8 minutes, filtering, and standing to obtain the heat insulation coating for the heat exchanger. The prepared heat insulation coating for the heat exchanger has good heat insulation, water resistance and salt spray resistance.

The invention relates to the technical field of lubricating oil additives, and discloses an environment-friendly additive for replacing a phosphorus-chlorine antiwear agent.The preparation method comprises the following steps that base oil is added into a reaction kettle, stirring is conducted for 15-20 min at the temperature of 50-70 DEG C at the speed of 300-600 rpm, then molybdenum oleate, modified hydrotalcite, modified eugenol and octyl dimethylbenzene are sequentially added under continuous stirring, uniform mixing is conducted, and the additive is obtained. The environment-friendly additive for replacing the phosphorus-chlorine anti-wear agent is obtained. Under high temperature and high pressure generated by friction, molybdenum oleate can be decomposed to form a molybdenum disulfide solid lubricating film with low shear strength, so that the wear resistance of the additive is enhanced; stearic acid is used for modifying hydrotalcite, so that the anti-wear effect is synergistically enhanced; an organic silicon chain segment in the modified eugenol can provide auxiliary lubrication, and polar groups are adsorbed on the metal surface, so that the corrosion resistance of the additive is improved; and the additive does not contain phosphorus, chlorine and other harmful elements, and accords with the development direction of modern green manufacturing and environment-friendly lubrication.

The invention relates to a natural latex / graphene aerogel composite material for oil-water separation and a preparation method thereof. The preparation method comprises the following steps: firstly, preparing graphene oxide by an improved Hummers method, and then preparing the natural latex / graphene aerogel by combining a hydrothermal self-assembly method, a bubble template method and a freeze-drying method. And then adjusting the use amount of the natural latex and process parameters to optimize the performance of the natural latex / graphene aerogel, thereby preparing the natural latex / graphene aerogel with optimal performance. The preparation method has the beneficial effects that the problem of oil-water separation performance is solved, excellent adsorption performance is shown on organic reagents (ethanol, n-butane, liquid paraffin, trichloromethane, xylene, kerosene, edible oil, cyclohexane and the like), and the adsorption range is 43.82-189.86 g / g; after 10-20 times of cycle tests, the thickness recovery rate and the absorption capacity are still 92% or above of the initial value.

The utility model is applicable to the technical field of dimethylbenzene production and processing equipment, and provides a dimethylbenzene production and processing mixer convenient to observe, which comprises a mixing tank, and a circulating observation component is mounted on one side wall of the mixing tank. According to the utility model, a group of circulating observation mechanism consisting of the circulating pump, the circulating pipe and the glass pipe is designed, so that in the stirring and mixing process, the circulating pump can enable mixed raw materials to circularly flow in the circulating pipe, and a worker can observe the overall mixing degree of the raw materials through the glass pipe in the flowing process; meanwhile, a driving motor drives an auxiliary gear to rotate through a main gear, so that the main gear and the auxiliary gear simultaneously drive five groups of rotating shafts and stirring blades to rotate to stir the raw materials, and the area of a stirring area can be effectively increased; raw materials can be stirred and mixed in all directions, and the mixing effect and observation performance of the device are effectively improved.

The reagent for detecting MHC-II expression of tumor cells in gastric cancer tissue comprises the following components in parts by mass: 10-30 parts of paraffin section preparation liquid, 2-10 parts of dewaxing liquid, 2-10 parts of sodium citrate antigen repair liquid, and 20-40 parts of immunohistochemical staining liquid; the dewaxing liquid comprises dimethylbenzene, and at least one of flavonol aminobenzoate derivative and sinapamide benzyl trimethylammonium benzoate salt; the flavonol aminobenzoate derivative has a nitrogen-containing group and a benzene ring, and the sinapamide benzyl trimethylammonium benzoate salt has a long-chain unsaturated alkane and a nitrogen-containing group. The reagent for detecting MHC-II expression of tumor cells in gastric cancer tissue can obtain high-quality immunohistochemical staining sections, thereby improving the sensitivity and specificity of MHC-II expression detection.

The invention discloses a CO2 response type gemini imidazoline surfactant and application thereof in fracturing fluid, tetraethylenepentamine and long-chain fatty acid are fed, dimethylbenzene with the mass equal to that of the long-chain fatty acid is used as a water carrying agent, the temperature is raised to 125-140 DEG C for reflux, then the temperature is continuously raised to 190-220 DEG C for reflux, the temperature is sequentially reduced to room temperature, and the CO2 response type gemini imidazoline surfactant is obtained. A gemini imidazoline viscous liquid is obtained; and step 2, dropwise adding a composition solution of 3-chloro-2-hydroxypropyl trimethyl ammonium chloride and acetone with the same mass into the gemini imidazoline in the step 1 while stirring, then adding an acid-binding agent with the same mole, reacting at room temperature, heating to 56-60 DEG C, distilling out acetone, and thus obtaining the CO2 response type gemini imidazoline surfactant. The surfactant can be used as a thickening agent of the clean fracturing fluid, the viscoelasticity of the clean fracturing fluid prepared by using the surfactant as the thickening agent is improved, and the formed clean fracturing fluid shows relatively strong acidity and can corrode inorganic blockages such as carbonic rock in part of a stratum.

The application discloses a preparation method of a high entanglement and fatigue resistant polyolefin thermoplastic elastomer, and the material is prepared from the following raw materials: 100 parts of ETPO elastomer, 1-35 parts of ETPO-UHMWPE solution blending masterbatch, 1-10 parts of vinyl boron-containing crosslinking agent, 0.05-0.2 parts of antioxidant and 0.01-5 parts of initiator. First, the ETPO-UHMWPE solution blending masterbatch A is prepared by using hot dimethylbenzene; second, the vinyl boron-containing crosslinking agent B is prepared by using 1,4-benzene diboronic acid and 3-allyloxy-1,2 propanediol; then, the ETPO, the masterbatch A, the vinyl boron-containing crosslinking agent B, the antioxidant and the initiator are mixed in a mixer or an extruder; finally, the material is formed by secondary processing in a conventional polymer processing mode. The application creatively realizes the synergy of chain entanglement and vitrimer network, improves the tensile strength, fatigue resistance and use temperature, has the advantages of simple operation process, low production cost and repeatable processing, and adopts conventional polymer processing equipment, and has the industrial application potential.