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119results about How to "Suitable for large-scale production applications" patented technology

Dye-sensitized nanocrystalline thin film solar cell with light trapping structure

The invention discloses a dye-sensitized nanocrystalline thin film solar cell with a light trapping structure. The dye-sensitized nanocrystalline thin film solar cell with the light trapping structure comprises a photo-anode, electrolyte and a counter electrode, wherein the photo-anode mainly comprises a conductive substrate and a nanocrystalline film; the nanocrystalline film consists of at least one layer of unit thin film; each layer of unit thin film is formed by laminating more than three layers of nanocrystalline thin films with different refractive indexes; and the light refractive indexes of the nanocrystalline thin films of the outmost layers on the two sides of the unit thin film are lower than the light refractive index of each nanocrystalline thin film of the inner layer of the unit thin film, and the light refractive indexes of each nanocrystalline thin film of the inner layer are gradually increased or gradually increased and then gradually decreased along a light projection direction. The cell provided by the invention fulfills the aim of trapping light by the scattering and complete reflection of light, is prepared from a wide range of materials by a simple preparation method, has a wide application range and can greatly enhance the light absorption and utilization of the thin films, thereby greatly optimizing the photoelectric conversion efficiency of the cell.
Owner:NANJING UNIV OF TECH

Method for recovering rhenium from molybdenum smelting waste acid

The invention discloses a method for recovering rhenium from molybdenum smelting waste acid and belongs to the technical field of metal rhenium recovery and recycle. The method comprises 1, filtering molybdenum smelting waste acid, and treating the filtrate by a composite aminoethylene weak basic anion exchange resin column for adsorption until adsorption is saturated, and 2, carrying out desorption on the saturated anion exchange resin column, collecting the desorption liquid and carrying out evaporation crystallization to obtain ammonium perrhenate. The composite aminoethylene weak basic anion exchange resin has large saturation adsorption quantity. The desorption liquid has rhenium content 100 times or more that of waste acid. Compared with the existing extraction method and ion exchange method, the method provided by the invention has a high rhenium recovery rate of 98% or more. Through use of solubility difference of ammonium perrhenate, ammonium molybdate and ammonium sulfate, ammonium perrhenate is purified by evaporation crystallization and ammonium perrhenate purity is 99.9% or more. The method has a simple rhenium recovery process, is environmentally friendly, is convenient for operation and is suitable for large scale production.
Owner:ZHENGZHOU MINERALS COMPOSITIVE UTILIZATION RES INST CHINESE GEOLOGICAL ACAD +1

Degradation bacterium for oil-base drilling cuttings, and preparation method and application method thereof

The invention discloses a degradation bacterium for oil-base drilling cuttings, and a preparation method and an application method thereof, and belongs to the technical field of microbiological processing of oil-containing solid wastes. The degradation bacterium for oil-base drilling cuttings is composed of multiple microorganisms, and is prepared by performing fermentation culturing on three degradation single bacteria which are obtained by performing enriching, separation, purification and screening on bacteria in petroleum polluted soil. The degradation bacterium for oil-base drilling cuttings comprises pPseudomonas aeruginosa, kocuria kristinae and acinetobacter calcoaceticus, is used for degradation of petroleum composition in oil-base drilling cuttings, and has the substantial advantages of high oil removal efficiency and short processing period. When oil-base drilling cutting with the initial oil content less than 5% is processed by using the degradation bacterium for 5-30 d, the oil content can be reduced to 1% or less, and the oil removal rate can reach 80% or more. The degradation bacterium also has good application prospect when being applied to biological restoration of oil-containing soil and oil-containing sludge.
Owner:CHINA PETROCHEMICAL CORP +1

Method for preparing negative pole slurry for lithium ion batteries

The invention discloses a method for preparing negative pole slurry for lithium ion batteries, which comprises the following steps of: 1, stirring a conductive agent, a dispersing agent and a solvent at a constant speed, so that a mixture is formed after the conductive agent, the dispersing agent and the solvent are completely dissolved; 2, adding a binder solution into the mixture, and then stirring the obtained object; 3, continuing to add a negative active material into the mixture, and then stirring the obtained object; 4, continuing to add a solvent into the mixture, and then uniformly stirring the obtained object; and 5, placing the mixture in a vacuum environment so as to finally obtain uniform negative pole slurry. According to the method for preparing negative pole slurry for lithium ion batteries, disclosed by the invention, the working efficiency of preparing the negative pole slurry for lithium ion batteries can be obviously improved, and the uniformity and stability of the negative pole slurry can be guaranteed; and meanwhile, the reduction of the production cost is facilitated, and the performance of lithium ion batteries is improved finally, therefore, the method is suitable for large-scale production applications and facilitates the improvement of the market application prospects of products of battery manufacturers.
Owner:TIANJIN LISHEN BATTERY

Sodium alginate-hydroxyapatite hybridization nano particle and preparing method thereof

The invention relates to a sodium alginate-hydroxyapatite hybridization nano particle. The sodium alginate-hydroxyapatite hybridization nano particle comprises, by mass, 65%-99.5% of hydroxyapatite and 0.5%-35% of sodium alginate, the sodium alginate-hydroxyapatite hybridization nano particle is in a needle shape, the length of the needle ranges from 10 nm to 70 nm, and the width of the needle ranges from 3 nm to 20 nm. A preparing method includes the steps that alginic acid polysaccharide is dissolved into deionized water to obtain an alginic acid polysaccharide solution with the mass concentration ranging from 0.2% to 0.8%, a calcium salt aqueous solution and a phosphate aqueous solution are added into alginic acid polysaccharide solution under stirring, and the adding amount of the calcium salt aqueous solution and the phosphate aqueous solution is determined with the molar ratio of Ca / P in a reaction system being (1-2.0):1 as a limit; and in addition, the volume ratio of the calcium salt aqueous solution to the phosphate aqueous solution is 1:(20-40), then the pH value of the reaction system is adjusted to be 10-12, stirring is stopped, standing ageing is carried out for at least 5 days, and a reaction product is collected after standing ageing is carried out and is dried. The sodium alginate-hydroxyapatite hybridization nano particle is particularly suitable for serving as an anti-cancer drug carrier.
Owner:SICHUAN UNIV

Special spherical calcium carbonate for stone paper and preparation method of special spherical calcium carbonate

The invention discloses special spherical calcium carbonate for stone paper and a preparation method of the special spherical calcium carbonate and provides spherical calcium carbonate which has the good liquidity in a heated state. The spherical calcium carbonate is formed by polymerizing caprolactam after the caprolactam infiltrates into micro-pores in the spherical calcium carbonate surface. A liquid infiltrates into the spherical tiny calcium carbonate surface under the action of high-pressure push of a high-pressure expansion fluid device, and energy accumulated on the spherical tiny calcium carbonate surface is released and expanded quickly due to sudden pressure release, so that the micro-pores are formed in the calcium carbonate surface, and spherical heavy calcium carbonate of the micro-pores in the surface adsorbs the caprolactam and is polymerized to form the spherical calcium carbonate with a caprolactam polymer inlaid in the surface. When the spherical calcium carbonate is used for processing raw materials of the stone paper, the processing fluidity and the dispersity of the stone paper are substantially improved due to the spherical characteristic of the calcium carbonate and the easy-plasticizing characteristic of the caprolactam polymer, and the good processing fluidity of the stone paper can be realized under the condition that a lubrication additive is reduced or not used.
Owner:JIANGSU XIYI HIGH NEW DISTRICT TECH DEV CO LTD

Mineral fiber softening agent

The invention discloses a mineral fiber softening agent. The mineral fiber softening agent is prepared from the following raw materials in part by weight: 40-55 parts of vinyl acetate-ethylene copolymer emulsion, 15-25 parts of vital gluten, 5-15 parts of inorganic adhesives, 3-5 parts of chlorinated polyethylene emulsion, 0.5-2 parts of organic adhesives and 0.2-0.5 part of silane unsaturated monomer. The vital gluten, the inorganic adhesives and the organic adhesives are subjected to compound modification in an acylation manner, by a strong polarity polar group of the chlorinated polyethylene emulsion, the obtained softening agent has high-permeation adhesion on mineral fibers, permeates in the fibers and firmly wraps surfaces of the mineral fibers, and owing to viscoelasticity of the vital gluten, the mineral fibers have good flexibility. Because the softening agent contains the water-soluble inorganic adhesives, metal cation electrolytes are formed on surfaces of the mineral fibers when the mineral fibers are softened by the softening agent, potential difference is generated between the surfaces of the mineral fibers and surrounding liquid, particularly, a binding force of the mineral fibers and plant fibers is increased, when the plant fibers are replaced, the mineral fibers can be connected with the plant fibers, ionic bonds are formed by combination of ions, and bonding strength of the fibers is improved.
Owner:广州市朗尔化工助剂有限公司

Synthesis method and application of nanometer SiO2/CaO adsorbent

The invention relates to a synthesis method of a nanometer SiO2/CaO adsorbent. Calcium carbonate and nanometer SiO2 are subjected to ball mining, crushing and sieving; the specific surface area of the nanometer SiO2 is greater than 200m<2>/g, and the nanometer SiO2 includes but is not limited to precipitation method nanometer SiO2, vapor phase method nanometer SiO2, ZSM-5 molecular sieves, MCM-41 molecular sieves, MCM-48 molecular sieves, MCM-50 molecular sieves and SBA-15 molecular sieves; the calcium carbonate (through being metered by CaO mass) and the nanometer SiO2 are weighed and are subjected to solid phase mixing according to a mass ratio of (80:20) to (95:5); the mixture is calcined for 2 to 6h at 850 to 950 DEG C in inert gas atmosphere; after cooling, an adsorbent product is obtained; when the adsorbent product is used for a circulating fluidized bed, the fast CO2 gathering and the adsorbent regeneration can be realized. The method has the advantages that a solid phase mixing technology is used; a liquid phase reaction process with high energy consumption and high cost is avoided; the product adsorption speed is high; the adsorption quantity proportion can reach 85 percent or higher at a 20s fast adsorption stage; the high-temperature stability is high; the circulation adsorption capacity is great; the adsorption capacity can still reach 0.30g CO2/g of the adsorbent after 30 circulations; the method is suitable for the realization of mass application in the circulating fluidized bed.
Owner:TSINGHUA UNIV

Low-temperature gas phase hydrolysis equipment for preparing white carbon black by using silicon tetrachloride

The invention discloses low-temperature gas phase hydrolysis equipment for preparing white carbon black by using silicon tetrachloride. The low-temperature gas phase hydrolysis equipment comprises a feeding system, a gas carrier system, a gas phase hydrolysis system, a cyclone separation system, a primary deacidification system, a secondary deacidification system and a tertiary deacidification system. Silicon tetrachloride and pure water are continuously introduced according to a molar ratio of 1 : (4 to 8); uniform liquid drops are formed through an atomizing spray head and are vaporized after encountering high-temperature carrier gas, and reaction is carried out in a gas phase hydrolysis tower at 120 to 180 DEG C, so as to produce the white carbon black and hydrogen chloride gas; gas-solid separation of a mixed product is realized through the cyclone separation system, and then drying is performed for 4 hours at 160 DEG C to obtain a white carbon black product; a concentrated hydrochloric acid byproduct is recycled from hydrogen chloride mixed gas through the primary deacidification system and the secondary deacidification system; tail gas is subjected to treatment through the tertiary deacidification system so as to realize pollution-free emission. According to the low-temperature gas phase hydrolysis equipment disclosed by the invention, reaction energy consumption can be reduced, corrosion of the equipment is slowed, and the production cost is reduced; moreover, production capacity of the white carbon black of 100 to 200kg / d and the concentrated hydrochloric acid byproduct are achieved; the prepared white carbon black product is excellent in performance, and has wide production application prospects.
Owner:TSINGHUA UNIV

Preparation method and application of magnetic Co-V/C3N3 composite supporter particles

The invention discloses a preparation method and application of magnetic Co-V / C3N3 composite carrier particles. The method comprises the following steps: collecting degradation-resistant organic wastewater, adding a magnetic Co-V / C3N4 modified photocatalytic material, and feeding a proper amount of oxygen to initiate degradation reaction of degradation-resistant organic matters under the irradiation of electron beams; and after the reaction is finished, carrying out solid-liquid separation on the magnetic Co-V / C3N4 and a water body under the action of a magnetic field, wherein the supernate is treated water. When the bottom of the reactor needs to be dredged, the magnetic Co-V / C3N4 can be separated from sediments at the bottom under the action of a magnetic field, so that the loss of the catalyst is avoided. The preparation method is carried out at normal temperature and normal pressure, reaction conditions are mild, and the process is simple; the added photocatalytic functional material is environment-friendly and does not generate secondary pollution; the wastewater treatment process is short, the treatment effect is good, and the method is suitable for large-scale treatment of degradation-resistant organic wastewater.
Owner:湖北中和普汇环保科技有限公司

Water-soluble fertilizer synergist additive and preparation method thereof

InactiveCN104140332AAvoid the defects of fertilizer efficiency reductionHydrophilicFertilizer mixturesCalcium hydroxideSoil science
The invention discloses a water-soluble fertilizer synergist additive. The water-soluble fertilizer synergist additive comprises the following components in parts by weight: 70-80 parts of white carbon black, 15-20 parts of acrylate, 10-15 parts of polyvinyl alcohol, 1-2 parts of stabilizing agent, 0.2-0.5 part of initiating agent and 0.2-0.3 part of dispersing agent. By virtue of dry process interpenetrating network, three materials are interpenetrated and wound to form a stable polymer, and the original performance of the materials before interpenetrating is guaranteed; meanwhile, three hydrophilic, adsorbed and water-soluble materials can complement defects in properties each other, so that the water-soluble fertilizer synergist additive can meet hydrophilic, adsorption and water solubility properties when being applied to a water-soluble fertilizer. By virtue of interpenetrating network, water-soluble nutrients in the water-soluble fertilizer are adsorbed, especially acrylate and nutrient ions in the water-soluble fertilizer form a stable compound, nutrients are prevented from being lost, and excellent decomposition on calcium carbonate, calcium hydroxide and calcium phosphate in water is realized, so that efficiency of the water-soluble fertilizer is improved.
Owner:蒋浩
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