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53results about How to "Coating method is simple" patented technology

Synthetic method for preparing CdSe/CdS/ZnS core-shell structure quantum dots by acid assistance

InactiveCN104498039ASmall emission wavelength effectCoating method is simpleLuminescent compositionsOrganic acidParaffin oils
The invention discloses a synthetic method for preparing CdSe / CdS / ZnS core-shell structure quantum dots by acid assistance. The synthetic method comprises the following steps: synthesizing a CdSe core quantum dot solution in a paraffin oleic acid system, using cadmium oleate as a precursor of a shell layer CdS, using a sulfur source dissolved in liquid paraffin as a precursor of the shell layers CdS and ZnS, using a zinc source dissolved in the liquid paraffin as a precursor of the shell layer ZnS, adding an organic acid in a precursor of S, and dripping the organic acid into the core quantum dot solution, wherein the organic acid reinforces the activity of the precursors of the shell layers, reduces the surface ligands of the core quantum dot, promotes the growth of the CdS shell layer on the surface of the CdSe core quantum dot and achieves epitaxial coating; dripping the precursor of Zn to wrap the ZnS shell layer to obtain a CdSe / CdS / ZnS core-shell structure quantum dot solution. The synthetic method disclosed by the invention has the advantages that the CdSe / CdS / ZnS core-shell structure quantum dots can be synthesized in the atmosphere under a non-phosphor system, the raw materials are cheap, the reaction temperature is low, the growth of the shell layers is fast, the operation is simple and mass production is suitable.
Owner:HUBEI UNIV

High-performance nanofiltration composite membrane containing polymer coating layer

InactiveCN110496533AHigh retention rateControl Separation PerformanceReverse osmosisPolymer sciencePoly ether ether ketone
The invention relates to a preparation method of a high-performance nanofiltration composite membrane containing a polymer coating layer. The preparation method comprises following steps: a polymer coating layer is introduced onto the surface of a porous supporting membrane; solvent volatilization treatment is carried out; interface polymerization is carried out on the supporting material containing the polymer coating layer, wherein the monomers adopted in interface polymerization are polyamines and poly acyl chlorides; after interface polymerization reaction, heat crosslinking treatment is carried out; or before introduction of the polymer coating layer, interface polymerization reaction is carried out on the surface of the porous supporting membrane. The adopted porous supporting material is prepared from a polymer material such as polysulfones, polyethersulfones, polyether ether ketones, polycarbonates, polyvinylidene fluoride, polyacrylonitrile, polyethylene, polypropylene, or inorganic porous materials such as alumina and titanium dioxide ceramic materials. The preparation method is capable of avoiding the seesaw effect of permeability and interception performance of nanofiltration and reverse osmosis membranes, and obtaining the nanofiltration membrane high in permeability and retention rate. The preparation method is low in cost, and simple in operation, and great meaning in the field of membrane material wide applications and circular economy is achieved.
Owner:SHANGHAI ADVANCED RES INST CHINESE ACADEMY OF SCI

Anticoagulation, antibacterial, anti-adhesion, anti-anti-inflammation and lubricating copolymer coating material for surface of silicon rubber material and preparation method thereof

The invention provides an anticoagulation, antibacterial, anti-adhesion, anti-anti-inflammation and lubricating copolymer coating material for the surface of a silicon rubber material and a preparation method thereof. The material is a high molecular copolymer formed by polyelectrolyte and active ester; the polyelectrolyte is a zwitter-ion polyelectrolyte which is generated by polymerizing phosphate ammonium or carboxyl ammonia or sulphur ammonia zwitter-ion monomers. The monomers and active ester monomers of the prepared polyelectrolyte are directly mixed and polymerized, or a homopolymer ofone of the two monomers is prepared at first, the homopolymer is adopted as a chain transfer agent, and the other monomer is adopted as a polymer monomer to obtain the copolymer. The prepared copolymer coating can be bonded on the surface of silicon rubber through the single coating technology to form the stable polymer coating; the number and density of microorganisms and bacteria attached to thesurface of the modified silicon rubber material are remarkably decreased, and the anticoagulation, antibacterial, anti-adhesion and anti-anti-inflammation performance can be remarkably improved; thesurface of the silicon rubber is high in hydrophilicity, the friction coefficient is remarkably lowered, and the lubricating performance can be obviously enhanced.
Owner:NANJING NORMAL UNIVERSITY

Preparation method for abrasion-resistant super-hydrophobic coating

The invention provides a preparation method for an abrasion-resistant super-hydrophobic coating. The preparation method comprises the following steps that acrylates copolymer and BYK-333 are mixed jointly and stirred uniformly, then a blended solution of ethyl acetate and butyl acetate is added, and adipic acid / neopentyl glycol / trimellitic anhydride copolymer, acetyl tributyl citrate, and epoxy resin are sequentially added after stirring is carried out for a moment, nitrocellulose is added to obtain a solution A; and an aluminum sheet is placed on a spin coater, a nano silicon dioxide particlesolution is immediately coated in a spinning mode after spin coating is completed, and then drying is carried out to obtain the abrasion-resistant super-hydrophobic coating. Hydrophobic modified silicon dioxide insets in the surface or an inner hole of PMMA, so that a white abrasion-resistant coating with a static WCA of 168 degrees + / -0.9 degrees and a rolling angle of less than 1 degree is obtained. The abrasion-resistant super-hydrophobic coating has the advantages of good self-cleaning effect, anti-icing and acid-alkali-resistant properties and capable of being applied to different substrates, and the above advantages provides a certain reference value for the industrial market requirement that super-hydrophobic materials has a certain mechanical stability and environmental adaptability.
Owner:CHINA THREE GORGES UNIV

Plasma resonance tilted fiber Bragg grating hydrogen sensor, detection system and method

The invention discloses a plasma resonance tilted fiber Bragg grating hydrogen sensor, a plasma resonance tilted fiber Bragg grating hydrogen detection system and a plasma resonance tilted fiber Bragg grating hydrogen method. The system comprises a light source, a polarizer, a polarization controller, a plasma resonance tilted fiber Bragg grating hydrogen sensor, a photoelectric detector, an oscilloscope and a gas storage container; the light source, the polarizer, the polarization controller, the hydrogen sensor, the photoelectric detector and the oscilloscope are sequentially connected with one another; the hydrogen sensor is arranged in the gas storage container when hydrogen is measured; the hydrogen sensor comprises an optical fiber engraved with a tilted fiber Bragg grating; the tilt angle of the tilted fiber Bragg grating is smaller than or equal to 45 degrees; the outer surface of the cladding layer of the optical fiber is plated with a nano-scale palladium film; plasma resonance waves on the surface of the palladium film are excited through the tilted fiber Bragg grating plated with the palladium film, so that specific recognition is carried out on the hydrogen; and the high-precision measurement of the static concentration and dynamic concentration change of the hydrogen is further realized.
Owner:JINAN UNIVERSITY

Method for covering plastic film on surface of wood or plastic special-shaped substrate

The invention discloses a method for coating a plastic film on the surface of woody or plastic deformed basis material, which relates to a method for coating a plastic film. The method solves the problems that the prior method for coating a plastic film influences the exterior quality of a product, the cost of the paint spraying on the surface of the woody basis material is high, and the noxious substance volatilized from the paint is easy to pollute the environment. The inventice method has the following steps that: firstly, plastic heat shrinking material is made into a cylindrical film; secondly, vacuum suction plastic is sprayed on the surface of the woody or the plastic profile basis material; thirdly, the cylindrical film made of the plastic heat shrinking material in the step one is covered on the outer surface of the gummed woody or the gummed plastic profile basis material prepared in the step two; fourthly, the woody or the plastic profile basis material processed through the step three is put into a vacuum sucking and coating machine to perform the contraction and the vacuum sucking and coating, and then the woody or the plastic profile basis material with the plastic film covered on the surface is obtained. The surface of the woody or the plastic profile basis material covered in the invention has no seam, the coating method is simple, and the production cost and the production cycle are reduced.
Owner:施永志

Method for plating thin film on inner wall of slender pipeline

The invention discloses a method for plating a thin film on an inner wall of a slender pipeline, belonging to the technical field of vacuum film plating. The method comprises the steps of: putting a pipeline to be plated with a film in a reaction chamber, alternatively introducing a gaseous phase precursor to a reactor in a pulse form, wherein the first precursor reaches to the inside of the pipeline and is chemically adsorbed on the inner wall of the pipeline to form a single adsorption layer; introducing a second precursor to react with the first precursor so as to generate a thin film with a single atom layer on the inner wall of the pipeline; cleaning the reactor through inert gas between every two precursor pulses, and repeating the adsorption and reaction processes to generate the thin film layer by layer. The method is used for plating the thin film on the inner wall of the slender pipeline in a gas adsorption and reaction combination manner to solve the problem that the thin film cannot be plated on the inner wall of the slender pipeline in a vacuum film plating method currently; and the method can be used for plating such thin film materials as metal, oxide, nitride, sulfide and fluoride, and the like so as to meet different demands.
Owner:NO 510 INST THE FIFTH RES INST OFCHINA AEROSPAE SCI & TECH

Method for preparing anti-icing self-repaired coating

The invention relates to a method for preparing a nano porous coating. The method comprises the following steps: mixing and stirring micron-order calcium carbonate particles, nano-grade silicon dioxide particles, polydimethylsiloxane and ethyl acetate so as to obtain an emulsion for later use; soaking a substrate into the emulsion, taking out the substrate after 10-20 minutes of soaking, and performing drying, namely drying the substrate with the coating for 50-80 minutes at 120-150 DEG C; and soaking the dried sample into diluted hydrochloric acid for 5-10 minutes, washing the dried sample with deionized water, and performing drying for 0.5-1.5 hours at 120-160 DEG C, so as to obtain an anti-icing self-repaired coating. A double-rough composite coating of a lotus leaf structure is prepared by mainly using a physical mixing and chemical corrosion methods, and the coating has good super-hydrophobicity under a low temperature condition, and thus has an anti-icing capability. The super-hydrophobicity coating prepared by using the method not only has good super-hydrophobicity and anti-icing capabilities, but also has a self repairing capability and acid-alkali resistance. The coating is low in preparation method cost, convenient to operate and wide in application substrate.
Owner:CHINA THREE GORGES UNIV

Core-shell composite positive electrode material coated with mixed polymer, its preparation method and application in lithium ion battery

The invention discloses a mixed polymer-coated core-shell composite positive electrode material, a preparation method thereof and application in a lithium ion battery. The composite positive electrodematerial comprises a positive active material core and a mixed polymer shell, wherein the mixed polymer shell is coated on a surface of the core and comprises a mixture of a conductive polymer and anorganic solid polymer. The method comprises the steps of 1) mixing polyethylene oxide and lithium hexafluorophosphate, and performing ball-milling to obtain a mixture A; 2) mixing the positive activematerial and a coupling agent, and performing dry ball-milling to obtain a mixture B; and 3) mixing the mixture A, the mixture B and the conductive polymer, and performing dry ball-milling and calcination to obtain the core-shell composite positive electrode material. The coating layer of the composite positive electrode material can be compatible with electron conductivity and lithium ion conductivity of the material, the internal resistance of the electrode material is effectively reduced, moreover, two materials in the coating layer are high in compatibility, and the coating uniformity isimproved.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

A kind of surface coating method of positive electrode material of lithium ion battery

The invention discloses a surface coating method of a cathode material for a lithium-ion battery. The method comprises the following steps: adding the cathode material for the lithium-ion battery to a magnesium salt solution, simultaneously adding a certain amount of lithium compound, carrying out ultrasound for 30-180 minutes, stirring the solution at 50-80 DEG C until dry, and putting the sample into a drying oven at 80 DEG C for drying; slowly heating the dried sample to 110-130 DEG C in a tube furnace, maintaining the temperature for 1-2 hours, heating the sample to 500-600 DEG C at the speed of 2 DEG C / min, maintaining the temperature for 2 hours, and introducing an oxidizing atmosphere to the tube furnace in the overall process; and burning the sample in the tube furnace. According to the cathode material for the lithium-ion battery, oxide coating is combined with carbon coating; and the amount of the oxide can be reduced, so that reduction of the conductivity caused by the oxide coating is well improved; meanwhile, reduction of the tap density caused by traditional carbon coating can also be improved; and the rate capability and the cycle performance of the material are improved. The carbon coating is carried out on the cathode material for the lithium-ion battery by a catalysis method; the coated carbon is uniform and controlled in thickness; and meanwhile, reduction of the cathode material caused by coated carbon can be reduced.
Owner:HEFEI GUOXUAN HIGH TECH POWER ENERGY

Lithium-ion battery ternary material coated with metal oxide on surface and preparation method thereof

The invention discloses a ternary cathode material coated with metal oxide on the surface and used for a lithium ion battery, and a preparation method for the ternary cathode material. The preparation method comprises the following steps: step 1, adding soluble metal salt to a dispersant solution to enable the salt to be sufficiently dispersed evenly; step 2, adding a cathode material in a solution obtained in the step 1 for stirring for 1-5 h; step 3, adding an aqueous solution of an alkali metal hydroxide to a solution obtained in the step 2, adjusting the pH value of the solution to be 7-12, and carrying out filtering and drying to obtain a cathode material coated with metal oxide on the surface; step 4, performing heat treatment on the cathode material coated with metal oxide on the surface at the temperature of 400-700 DEG C to obtain the ternary cathode material coated with metal oxide on the surface. According to the preparation method for the ternary cathode material coated with metal oxide on the surface and used for the lithium ion battery, the method is simple, polyacrylamide is introduced as a dispersing agent and a flocculating agent, so that uniform coating of the ternary cathode material is realized, industrial production is facilitated, and the performance of the modified ternary cathode material is greatly improved.
Owner:SHANGHAI INST OF SPACE POWER SOURCES

Coating method of woven artificial blood vessel and artificial blood vessel

The invention belongs to the technical field of medical instruments, and particularly relates to a coating method of a woven artificial blood vessel and the woven artificial blood vessel. According to the method, a step-by-step coating mode is adopted, the braided tube blank is firstly coated, and the coating is performed under the flat state of the tube blank, so that the contact surface tension of the coating solution and the artificial blood vessel is consistent, the uniformity of the coating is solved, and meanwhile, the water permeation amount of the artificial blood vessel is also effectively reduced; according to the artificial blood vessel and the preparation method thereof, the artificial blood vessel prepared by the method is uniform in coating, small in overall water permeation amount and good in biocompatibility, good elasticity and compliance of the artificial blood vessel are maintained, and the artificial blood vessel has the advantages of being simple in process, convenient to operate, low in cost and good in application prospect. The prepared artificial blood vessel is stored after sterilization, does not need to be pre-coagulated before implantation, and can be directly used for clinical transplantation after being soaked in normal saline.
Owner:山东欣脉通生物科技有限公司 +2

Hemispherical glass outer surface film coating device and method

The invention relates to a hemispherical glass outer surface film coating device and method. The hemispherical glass outer surface film coating device comprises a film coating cavity, a film coating mechanism, an adjustable fixing mechanism and a rotating mechanism. The film coating mechanism is arranged in the film coating cavity and used for conducting the film coating technology on multiple circular ring surfaces in sequence. The adjustable fixing mechanism is arranged on the film coating cavity, and the position of the adjustable fixing mechanism can be adjusted according to the film coating position of a piece of hemispherical glass. The rotating mechanism is connected with the adjustable fixing mechanism in a pivot joint mode and can be driven by the adjustable fixing mechanism to adjust the position of the rotating mechanism. The rotating mechanism is used for achieving the process that when the film coating technology is conducted, the rotating mechanism is connected with the hemispherical glass, drives the hemispherical glass to rotate, controls the multiple circular ring surfaces to face the film coating mechanism in sequence by rotating around the pivot joint end of therotating mechanism, and conducts the film coating technology on the multiple circular ring surfaces in sequence. According to the hemispherical glass outer surface film coating device and method, thehemispherical glass is divided into the multiple circular ring surfaces, the multiple circular ring surfaces are subjected to the film coating technology in sequence, and therefore the whole film coating process can be accomplished only through one cathode.
Owner:JIANGSU IRON ANCHOR GLASS LTD BY SHARE LTD
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